Table 4.
LC-MS/MS conditions and parameters for program 2
| Name | MRM | Dwell (s) | CV (V) | CE (V) | Mode | Retention time (min) | Time window ± (min) | Performance |
|---|---|---|---|---|---|---|---|---|
| Citrate (Cit) | 191 → 111 | 0.006 | 20 | 10 | ESI- | 1.2 | 0.1 | ∗ |
| α-Ketoglutarate (αKG) | 145 → 101 | 0.006 | 20 | 6 | ESI- | 1.1 | 0.2 | ∗∗ |
| Succinate (Suc) | 117 → 73 | 0.006 | 24 | 12 | ESI- | 0.72 | 0.1 | ∗∗ |
| Fumarate (Fum) | 115 → 71 | 0.006 | 18 | 8 | ESI- | 0.68 | 0.1 | ∗∗ |
| Malate (Mal) | 133 → 115 | 0.006 | 20 | 10 | ESI- | 1.05 | 0.2 | ∗∗ |
| Oxaloacetate (Oaa) | 131 → 87 | 0.006 | 40 | 10 | ESI- | 0.78 | 0.1 | ∗ |
| Pyruvate | 86.9 → 42.9 | 0.006 | 18 | 8 | ESI- | 0.77 | 0.1 | ∗∗ |
| Lactate | 89 → 43 | 0.006 | 20 | 10 | ESI- | 0.79 | 0.1 | ∗∗∗ |
| Nicotinic acid adenine dinucleotide phosphate (NAADP) | 745 → 604 | 0.006 | 30 | 10 | ESI+ | 0.56 | 0.1 | ∗ |
| Nicotinamide adenine dinucleotide phosphate (NADP) | 744 → 604 | 0.006 | 26 | 18 | ESI+ | 4.68 | 0.3 | ∗ |
| Reduced nicotinamide adenine dinucleotide (NADH) | 666 → 649 | 0.006 | 26 | 20 | ESI+ | 4.66 | 0.3 | ∗ |
| Nicotinic acid adenine dinucleotide (NAAD) | 665 → 428 | 0.006 | 24 | 24 | ESI+ | 4.21 | 0.15 | ∗ |
| Nicotinamide adenine dinucleotide (NAD+) | 664 → 428 | 0.006 | 26 | 26 | ESI+ | 4.15 | 0.15 | ∗∗ |
| Adenosine 5′-diphosphate (ADP) | 428 → 136 | 0.006 | 30 | 26 | ESI+ | 4.2 | 0.15 | ∗ |
| Inosine monophosphate (IMP) | 349 → 137 | 0.006 | 14 | 22 | ESI+ | 3.85 | 0.2 | ∗∗ |
| Adenosine 5′-monophosphate (AMP) | 348 → 136 | 0.006 | 30 | 30 | ESI+ | 3.88 | 0.1 | ∗∗∗ |
| Uridine monophosphate (UMP) | 325 → 97 | 0.006 | 20 | 12 | ESI+ | 3.72 | 0.2 | ∗ |
| Cytidine monophosphate (CMP) | 324 → 112 | 0.006 | 16 | 22 | ESI+ | 3.91 | 0.1 | ∗∗∗ |
| Uridine | 245 → 113 | 0.006 | 18 | 16 | ESI+ | 1.01 | 0.1 | ∗∗∗ |