Table 8.
LC-MS/MS conditions and parameters for program 4
Name | MRM | Dwell (s) | CV (V) | CE (V) | Mode | Retention time (min) | Time window ± (min) | Performance |
---|---|---|---|---|---|---|---|---|
16:0 Lyso PA | 409 → 153 | 0.009 | 30 | 30 | ESI- | 5.86 | 0.2 | ∗∗ |
18:0 Lyso PA | 437 → 153 | 0.009 | 30 | 32 | ESI- | 5.83 | 0.2 | ∗∗ |
18:1 Lyso PA | 435 → 153 | 0.009 | 30 | 33 | ESI- | 5.84 | 0.2 | ∗∗ |
18:2 Lyso PA | 433 → 153 | 0.009 | 30 | 30 | ESI- | 5.87 | 0.3 | ∗∗ |
20:4 Lyso PA | 457 → 153 | 0.009 | 30 | 30 | ESI- | 5.85 | 0.2 | ∗∗ |
16:0 Lyso PC | 496.5 → 184.2 | 0.009 | 30 | 30 | ESI+ | 6.02 | 0.15 | ∗∗∗ |
18:0 Lyso PC | 524.6 → 184.2 | 0.009 | 30 | 30 | ESI+ | 5.96 | 0.15 | ∗∗∗ |
18:1 Lyso PC | 522.6 → 184.2 | 0.009 | 30 | 30 | ESI+ | 5.97 | 0.15 | ∗∗∗ |
18:2 Lyso PC | 520.6 → 184.2 | 0.009 | 30 | 30 | ESI+ | 6.03 | 0.15 | ∗∗∗ |
20:4 Lyso PC | 544.6 → 184.2 | 0.009 | 30 | 30 | ESI+ | 6.01 | 0.15 | ∗∗∗ |
34:1 PC | 760.7 → 184.2 | 0.009 | 30 | 30 | ESI+ | 5.71 | 0.1 | ∗∗∗ |
34:2 PC | 758.7 → 184.2 | 0.009 | 30 | 30 | ESI+ | 5.7 | 0.1 | ∗∗∗ |
36:2 PC | 786.7 → 184.2 | 0.009 | 30 | 30 | ESI+ | 5.69 | 0.1 | ∗∗∗ |
36:3 PC | 784.7 → 184.2 | 0.009 | 30 | 30 | ESI+ | 5.68 | 0.1 | ∗∗∗ |
36:4 PC | 782.7 → 184.2 | 0.009 | 30 | 30 | ESI+ | 5.69 | 0.1 | ∗∗∗ |