Table 2. CCD Experimental Matrix and Experimental Results for This Study.
| run | n(glu)/n(V) | concentration of H2SO4 | reaction time/min | reaction temperature/°C | adsorption efficiency/% |
|---|---|---|---|---|---|
| 1 | 1.5 | 10 | 35 | 30 | 3.61 |
| 2 | 1.5 | 20 | 10 | 30 | 63.88 |
| 3 | 1.5 | 20 | 60 | 30 | 5.42 |
| 4 | 3.0 | 20 | 35 | 30 | 10.90 |
| 5 | 0.0 | 20 | 35 | 30 | 4.55 |
| 6 | 1.5 | 30 | 35 | 30 | 5.29 |
| 7 | 0.0 | 10 | 35 | 60 | 27.05 |
| 8 | 1.5 | 10 | 10 | 60 | 73.40 |
| 9 | 1.5 | 10 | 60 | 60 | 35.57 |
| 10 | 3.0 | 10 | 35 | 60 | 66.59 |
| 11 | 1.5 | 20 | 35 | 60 | 22.70 |
| 12 | 3.0 | 20 | 60 | 60 | 42.73 |
| 13 | 3.0 | 20 | 10 | 60 | 27.14 |
| 14 | 1.5 | 20 | 35 | 60 | 36.75 |
| 15 | 1.5 | 20 | 35 | 60 | 36.75 |
| 16 | 0.0 | 20 | 10 | 60 | 20.31 |
| 17 | 1.5 | 20 | 35 | 60 | 36.75 |
| 18 | 0.0 | 20 | 60 | 60 | 9.36 |
| 19 | 1.5 | 20 | 35 | 60 | 36.75 |
| 20 | 1.5 | 30 | 60 | 60 | 5.42 |
| 21 | 1.5 | 30 | 10 | 60 | 13.48 |
| 22 | 0.0 | 30 | 35 | 60 | 6.30 |
| 23 | 3.0 | 30 | 35 | 60 | 7.17 |
| 24 | 1.5 | 10 | 35 | 90 | 90.72 |
| 25 | 1.5 | 20 | 60 | 90 | 76.79 |
| 26 | 0.0 | 20 | 35 | 90 | 61.82 |
| 27 | 3.0 | 20 | 35 | 90 | 81.61 |
| 28 | 1.5 | 20 | 10 | 90 | 70.12 |
| 29 | 1.5 | 30 | 35 | 90 | 57.44 |