Table 2. CCD Experimental Matrix and Experimental Results for This Study.
run | n(glu)/n(V) | concentration of H2SO4 | reaction time/min | reaction temperature/°C | adsorption efficiency/% |
---|---|---|---|---|---|
1 | 1.5 | 10 | 35 | 30 | 3.61 |
2 | 1.5 | 20 | 10 | 30 | 63.88 |
3 | 1.5 | 20 | 60 | 30 | 5.42 |
4 | 3.0 | 20 | 35 | 30 | 10.90 |
5 | 0.0 | 20 | 35 | 30 | 4.55 |
6 | 1.5 | 30 | 35 | 30 | 5.29 |
7 | 0.0 | 10 | 35 | 60 | 27.05 |
8 | 1.5 | 10 | 10 | 60 | 73.40 |
9 | 1.5 | 10 | 60 | 60 | 35.57 |
10 | 3.0 | 10 | 35 | 60 | 66.59 |
11 | 1.5 | 20 | 35 | 60 | 22.70 |
12 | 3.0 | 20 | 60 | 60 | 42.73 |
13 | 3.0 | 20 | 10 | 60 | 27.14 |
14 | 1.5 | 20 | 35 | 60 | 36.75 |
15 | 1.5 | 20 | 35 | 60 | 36.75 |
16 | 0.0 | 20 | 10 | 60 | 20.31 |
17 | 1.5 | 20 | 35 | 60 | 36.75 |
18 | 0.0 | 20 | 60 | 60 | 9.36 |
19 | 1.5 | 20 | 35 | 60 | 36.75 |
20 | 1.5 | 30 | 60 | 60 | 5.42 |
21 | 1.5 | 30 | 10 | 60 | 13.48 |
22 | 0.0 | 30 | 35 | 60 | 6.30 |
23 | 3.0 | 30 | 35 | 60 | 7.17 |
24 | 1.5 | 10 | 35 | 90 | 90.72 |
25 | 1.5 | 20 | 60 | 90 | 76.79 |
26 | 0.0 | 20 | 35 | 90 | 61.82 |
27 | 3.0 | 20 | 35 | 90 | 81.61 |
28 | 1.5 | 20 | 10 | 90 | 70.12 |
29 | 1.5 | 30 | 35 | 90 | 57.44 |