Table 3.
Recoveries and precision of four compounds spiked in different aquatic products (n = 3).
Analytes | Add Level(µg/kg) | Recovery/% (RSD/%) | ||||||||
---|---|---|---|---|---|---|---|---|---|---|
Bream | Trout | Grass Carp | Fresh Shrimps | Chinese Mitten Crab |
Crucian Carp | Perch | Catfish | Mussel | ||
MB | 1 | 93.2 (2.63) | 96.5 (4.27) | 95.2 (4.51) | 96.7 (7.04) | 89.9 (6.58) | 92.7 (3.04) | 91.5 (2.21) | 90.5 (4.18) | 89.7 (6.24) |
5 | 90.5 (5.23) | 95.0 (4.01) | 93.4 (3.28) | 95.1 (3.24) | 91.1 (5.63) | 93.3 (5.32) | 93.5 (3.08) | 96.0 (5.36) | 90.5 (6.06) | |
10 | 96.4 (6.37) | 95.3 (7.68) | 92.5 (4.05) | 97.5 (2.84) | 90.7 (6.70) | 90.5 (5.01) | 93.9 (4.29) | 93.2 (1.05) | 91.5 (5.71) | |
AZA | 1 | 86.2 (7.15) | 82.9 (7.52) | 88.9 (3.57) | 87.2 (6.35) | 83.2 (8.04) | 86.1 (3.82) | 88.6 (3.66) | 83.5 (6.01) | 81.6 (1.28) |
5 | 88.3 (8.63) | 84.9 (7.67) | 90.7 (3.69) | 84.9 (5.08) | 86.4 (8.36) | 83.1 (3.66) | 87.9 (2.08) | 85.5 (5.47) | 82.0 (1.38) | |
10 | 91.0 (5.72) | 89.5 (5.34) | 91.0 (2.61) | 86.5 (7.04) | 88.7 (6.04) | 88.6 (2.79) | 89.2 (1.99) | 83.9 (3.28) | 85.0 (1.98) | |
AZB | 1 | 95.3 (4.25) | 96.0 (5.05) | 97.1 (1.07) | 95.4 (5.60) | 92.5 (7.74) | 94.3 (1.35) | 92.8 (5.27) | 91.8 (2.04) | 93.4 (3.06) |
5 | 96.0 (3.35) | 94.2 (4.75) | 95.0 (2.67) | 96.2 (5.07) | 93.4 (6.66) | 90.5 (2.07) | 90.8 (3.31) | 93.0 (1.29) | 96.0 (1.08) | |
10 | 94.2 (3.07) | 93.8 (5.01) | 93.8 (1.96) | 93.7 (4.14) | 95.2 (4.24) | 92.0 (1.72) | 95.4 (3.07) | 91.2 (2.22) | 94.4 (1.66) | |
AZC | 1 | 73.2 (3.58) | 75.1 (5.05) | 74.5 (3.77) | 72.1 (5.74) | 71.8 (8.05) | 75.4 (4.76) | 74.8 (6.12) | 75.5 (7.22) | 72.1 (6.01) |
5 | 72.8 (4.57) | 77.0 (5.34) | 74.3 (3.04) | 75.4 (4.87) | 72.2 (6.80) | 73.5 (5.33) | 73.0 (5.76) | 72.0 (2.05) | 74.2 (5.20) | |
10 | 75.7 (3.39) | 78.7 (1.87) | 72.7 (3.30) | 72.7 (5.02) | 78.1 (6.17) | 78.6 (4.21) | 72.8 (3.35) | 74.6 (5.00) | 76.6 (6.45) |