Table 1.
Boiling Time (min) |
Yield | Particle Size | Organic Content |
Magnetic Properties (RT) | |||
---|---|---|---|---|---|---|---|
TEM | XRD | ||||||
Ρ (%) |
DTEM (nm) |
σTEM/DTEM (nm) |
DXRD (nm) |
Org (%) |
Ms (Am2/Kg) |
χ (Am2 Kg−1 T−1) |
|
5 | 37 ± 11 | 13 ± 2 | 0.33 ± 0.05 | 13.0 ± 0.2 | 9.6 ± 0.9 | 67.5 ± 0.2 | 940 ± 100 |
15 | 48 ± 18 | 14 ± 1 | 0.31 ± 0.03 | 13.3 ± 0.4 | 9.1 ± 0.4 | 65.3 ± 1.5 | 900 ± 100 |
30 | 56 ± 16 | 13 ± 2 | 0.36 ± 0.01 | 13.3 ± 0.7 | 11.1 ± 0.9 | 63.0 ± 2.1 | 800 ± 99 |
60 | 71 ± 10 | 16 ± 4 | 0.29 ± 0.05 | 13.7 ± 1.0 | 8.8 ± 0.2 | 65.7 ± 2.0 | 790 ± 72 |
120 | 61 ± 8 | 20 ± 1 | 0.23 ± 0.03 | 13.5 ± 0.6 | 11 ± 0.9 | 67.3 ± 1.8 | 870 ± 74 |
Unscaled sample | |||||||
30 | 24 ± 7 | 14 ± 4 | 0.27 ± 0.02 | 12.3 ± 0.4 | 14 ± 3 | 66 ± 2 | 1200 ± 120 |