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. 2021 Jul 31;19(8):439. doi: 10.3390/md19080439

Table 2.

13C NMR (150 MHz) data of compounds 13 in CD3OD.

Position δC, Type
1 2 3
1 (N) - - -
2 167.3 (C) 167.3 (C) 166.9 (C)
3 66.7 (CH) 67.0 (CH) 66.3 (CH)
4 (N) - - -
5 162.2 (C) 161.3 (C) 163.1 (C)
6 47.4 (CH2) n.o. 1 45.7 (CH2)
7 36.4 (CH2) 36.4 (CH2) 36.4 (CH2)
8 136.1 (C) 136.3 (C) 135.8 (C)
9 131.5 (CH) 131.5 (CH) 131.4 (CH)
10 129.7 (CH) 129.7 (CH) 129.8 (CH)
11 128.7 (CH) 128.7 (CH) 128.8 (CH)
12 129.7 (CH) 129.7 (CH) 129.8 (CH)
13 131.5 (CH) 131.5 (CH) 131.4 (CH)
1′ 173.2 (C) 172.9 (C) 175.8 (C)
2′ 39.1 (CH2) 39.2 (CH2) 38.9 (CH2)
3′ 58.1 (CH) n.o. 1 n.o. 1
4′ 31.4 (CH2) 31.6 (CH2) 31.4 (CH2)
5′ 27.2 (CH2) 27.4 (CH2) 27.1 (CH2)
6′–9′ 30.2-30.06 (CH2) 30.2-30.06 (CH2) 30.2-30.06 (CH2)
10′ 33.0 (CH2) 33.0 (CH2) 33.0 (CH2)
11′ 23.7 (CH2) 23.7 (CH2) 23.7 (CH2)
12′ 14.4 (CH3) 14.4 (CH3) 14.4 (CH3)
1″ 37.1 (CH2) 39.7 (CH2) -
2″ 29.8 (CH2) 27.7 (CH2) -
3″ 38.6 (CH2) 26.5 (CH2) -
4″ - 40.4 (CH2) -

1 n.o.: not observed.