Table 2.
Position | δC, Type | ||
---|---|---|---|
1 | 2 | 3 | |
1 (N) | - | - | - |
2 | 167.3 (C) | 167.3 (C) | 166.9 (C) |
3 | 66.7 (CH) | 67.0 (CH) | 66.3 (CH) |
4 (N) | - | - | - |
5 | 162.2 (C) | 161.3 (C) | 163.1 (C) |
6 | 47.4 (CH2) | n.o. 1 | 45.7 (CH2) |
7 | 36.4 (CH2) | 36.4 (CH2) | 36.4 (CH2) |
8 | 136.1 (C) | 136.3 (C) | 135.8 (C) |
9 | 131.5 (CH) | 131.5 (CH) | 131.4 (CH) |
10 | 129.7 (CH) | 129.7 (CH) | 129.8 (CH) |
11 | 128.7 (CH) | 128.7 (CH) | 128.8 (CH) |
12 | 129.7 (CH) | 129.7 (CH) | 129.8 (CH) |
13 | 131.5 (CH) | 131.5 (CH) | 131.4 (CH) |
1′ | 173.2 (C) | 172.9 (C) | 175.8 (C) |
2′ | 39.1 (CH2) | 39.2 (CH2) | 38.9 (CH2) |
3′ | 58.1 (CH) | n.o. 1 | n.o. 1 |
4′ | 31.4 (CH2) | 31.6 (CH2) | 31.4 (CH2) |
5′ | 27.2 (CH2) | 27.4 (CH2) | 27.1 (CH2) |
6′–9′ | 30.2-30.06 (CH2) | 30.2-30.06 (CH2) | 30.2-30.06 (CH2) |
10′ | 33.0 (CH2) | 33.0 (CH2) | 33.0 (CH2) |
11′ | 23.7 (CH2) | 23.7 (CH2) | 23.7 (CH2) |
12′ | 14.4 (CH3) | 14.4 (CH3) | 14.4 (CH3) |
1″ | 37.1 (CH2) | 39.7 (CH2) | - |
2″ | 29.8 (CH2) | 27.7 (CH2) | - |
3″ | 38.6 (CH2) | 26.5 (CH2) | - |
4″ | - | 40.4 (CH2) | - |
1 n.o.: not observed.