Table 1. Experimental details.
| Crystal data | |
| Chemical formula | [Fe(C5H5)(C18H13ClN)] |
| M r | 399.68 |
| Crystal system, space group | Orthorhombic, P b c a |
| Temperature (K) | 150 |
| a, b, c (Å) | 10.0991 (18), 7.7277 (14), 45.979 (8) |
| V (Å3) | 3588.3 (11) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 1.00 |
| Crystal size (mm) | 0.13 × 0.12 × 0.04 |
| Data collection | |
| Diffractometer | Bruker D8 QUEST PHOTON 3 diffractometer |
| Absorption correction | Multi-scan (TWINABS; Sheldrick, 2009 ▸) |
| Tmin, Tmax | 0.88, 0.96 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 12370, 4001, 2903 |
| R int | 0.046 |
| (sin θ/λ)max (Å−1) | 0.653 |
| Refinement | |
| R[F2 > 2σ(F 2)], wR(F 2), S | 0.063, 0.118, 1.17 |
| No. of reflections | 4001 |
| No. of parameters | 233 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.44, −0.38 |