Bruker SMART APEXII CCD diffractometer | 5344 independent reflections |
Radiation source: fine-focus sealed tube | 4453 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.034 |
ω scans | θmax = 28.3°, θmin = 1.5° |
Absorption correction: multi-scan (SADABS; Bruker, 2005) | h = −37→37 |
Tmin = 0.830, Tmax = 0.991 | k = −5→5 |
19760 measured reflections | l = −26→26 |