Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.055	Hydrogen site location: mixed
wR(F2) = 0.146	H atoms treated by a mixture of independent and constrained refinement
S = 1.18	w = 1/[σ2(Fo2) + (0.0612P)2 + 1.1713P] where P = (Fo2 + 2Fc2)/3
5344 reflections	(Δ/σ)max = 0.001
325 parameters	Δρmax = 0.31 e Å−3
0 restraints	Δρmin = −0.24 e Å−3