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. 2021 Mar 13;11(8):2362–2395. doi: 10.1016/j.apsb.2021.03.019

Table 3.

Synthesis methods of MOFs.

Method Advantage Disadvantage
Nonsolvothermal synthesis
  • • Under ambient pressure

  • • Simplifier synthetic requirements

  • • Long reaction time

  • • Low yield

  • • Large particle size

Solvothermal synthesis
  • • Higher yield than nonsolvothermal synthesis

  • • Smaller and more homogeneous crystals than nonsolvothermal synthesis

  • • Long reaction time

Microwave assisted solvothermal synthesis
  • • Environment-friendly rapid synthesis

  • • Morphology and size control

  • • High yield

  • • Good monodispersity

  • • Specific device

Sonochemical synthesis
  • • Easy and environment-friendly rapid synthesis

  • • Good monodispersity

  • • Further sonication led to decomposition of the crystals

  • • Low yield

Mechanochemical synthesis
  • • Solvent-free

  • • Low-cost and high-throughput production

  • • Energy and materials consumption

  • • Potential structure change

Electrochemical synthesis
  • • Prepare a higher solids content

  • • Specific device