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. 2021 Aug 25;6(35):22603–22615. doi: 10.1021/acsomega.1c02570

Table 1. Effect of a Solvent on the Sulfur Content in DEAE-Cellulose Sulfates during Sulfation with Sulfamic Acid in the Presence of Urea at 90 °C for 3.0 h.

no. solvent permittivity Kb sulfur content (wt %)
1 1,4-dioxane 2.3 1.2 × 10–17 10.1
2 pyridine 12.5 1.5 × 10–9 8.9
3 morpholine 7.3 2.1 × 10–6 7.2
4 piperidine 5.9 1.3 × 10–3 7.9
5 diglyme 7.4 2.0 × 10–18 9.4