Table 2. 13C NMR Spectroscopic Data of Compounds 1–5 in CD3OD.
position | GB (1) | 2 | 3 | 4 | 5 |
---|---|---|---|---|---|
1 | 75.5 | 75.5 | 80.5 | 43.6 | 79.3 |
2 | 93.3 | 95.2 | 88.4 | 83.9 | 98.7 |
3 | 84.7 | 84.8 | 86.7 | 87.4 | 60.5 |
4 | 100.2 | 100.7 | 104.1 | 104.0 | 96.7 |
5 | 69.2 | 68.2 | 78.5 | 73.9 | 75.8 |
6 | 80.7 | 81.4 | 84.0 | 93.6 | 82.5 |
7 | 38.1 | 37.8 | 36.5 | 36.8 | 37.0 |
8 | 50.5 | 54.8 | 58.8 | 58.2 | 55.1 |
9 | 73.5 | 73.3 | 70.3 | 68.8 | 68.5 |
10 | 70.7 | 71.2 | 72.0 | 72.9 | 71.4 |
11 | 175.2 | 177.3 | 174.7 | 174.5 | 177.3 |
12 | 111.9 | 110.9 | 110.6 | 111.5 | 110.1 |
13 | 172.7 | 175.1 | 176.3 | 176.2 | 179.4 |
14 | 43.3 | 43.9 | 41.5 | 41.2 | 40.3 |
15 | 178.4 | 180.2 | 179.6 | 179.7 | 176.8 |
16 | 8.1 | 8.1 | 13.9 | 14.2 | 16.2 |
17 | 33.3 | 34.3 | 34.6 | 34.5 | 34.3 |
18–20 | 29.5 | 30.6 | 30.5 | 30.5 | 30.7 |
1′ | 42.3 | 42.0 | 41.9 | 42.3 | |
2′ | 23.3 | 23.6 | 23.6 | 23.3 | |
3′ | 11.8 | 11.8 | 11.8 | 11.8 | |
1″ | 41.9 | 41.9 | 42.3 | ||
2″ | 23.5 | 23.5 | 23.0 | ||
3″ | 11.7 | 11.7 | 11.8 |