Table A1.
Synthesis of ADT-OH
| Reagent | C10H8OS3 (ADT) | C5H6NCl |
|---|---|---|
| M (g/mol) | 240.36 | 115.56 |
| m (g) | 10.5853 | 50.01 |
| n (mol) | 0.44 | 0.4327 |
| Melting point (℃) | 110 | −41.6 |
| Boiling point (℃) | — | 115.2 |
| Solvent | — | |
| Reaction temperature (℃) | 215 | |
| Reaction time(min) | 60 |
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