Table 1. Reaction Conditions.
entry | TfOH (equiv) | solvent | yield (%)a18c |
---|---|---|---|
1 | 1.0 | DCM (0.10 M) | 89 |
2 | 1.0 | PhMe (0.10 M) | 93 |
3 | 1.0 | PhMe (0.05 M) | 84 |
Isolated yield.
entry | TfOH (equiv) | solvent | yield (%)a18c |
---|---|---|---|
1 | 1.0 | DCM (0.10 M) | 89 |
2 | 1.0 | PhMe (0.10 M) | 93 |
3 | 1.0 | PhMe (0.05 M) | 84 |
Isolated yield.