Table 2.
Hydrogen bonds geometry in the crystal of [VOO(dipic)](2-phepyH)·H2O.
| D–H···A | d(D–H) [Å] | d(H···A) [Å] | d(D⋯A) (Å) | ∠D–H⋯A (°) |
|---|---|---|---|---|
| O1W–H1WA···O12 i | 0.95(2) | 1.91(2) | 2.811(3) | 158(4) |
| O1W–H1WB···O13 | 0.95(2) | 1.91(2) | 2.826(3) | 161(4) |
| N21–H21···O1W | 0.87(3) | 1.86(3) | 2.699(4) | 161(4) |
| C3–H3···O9 ii | 0.93 | 2.40 | 3.330(4) | 177 |
| C5–H5···O9 iii | 0.93 | 2.38 | 3.250(4) | 157 |
| C26–H26···O11 i | 0.93 | 2.35 | 3.135(4) | 142 |
| C28–H28···O1W | 0.93 | 2.44 | 3.345(4) | 165 |
| C29–H29···O14 | 0.93 | 2.58 | 3.389(5) | 145 |
Symmetry code: (i) x,½ − y, ½ + z; (ii) 1 − x,2 − y,1 − z; (iii) x,3/2 − y, − ½ + z.