Table 3.
Method performance parameters.
| Analyte | LOQ Solution (μg/L) | LOQ Maize (μg/kg) | RE (%) | SSE (%) | RA (%) | RSDr (%) |
|---|---|---|---|---|---|---|
| D3G (ext.) | <10 | <40 | 94.7 | 75.9 | 92.3 | 3.1 |
| D3G (int.) | 97.5 | 8.3 | ||||
| DON (ext.) | <10 | <40 | 101 | 86.4 | 104 | 5.9 |
| DON (int.) | 103 | 5.3 | ||||
| 15ADON (ext.) | <30 | <120 | 105 | 67.8 | 105 | 9.4 |
| 15ADON (int.) | 100 | 7.8 | ||||
| 3ADON (ext.) | <10 | <40 | 94.4 | 63.2 | 90.8 | 7.0 |
| 3ADON (int.) | 96.2 | 5.7 |
LOQ: limit of quantification; RE: extraction recovery; SSE: signal suppression or enhancement; RA: apparent recovery; RSDr: relative standard deviation under conditions of repeatability; ext. external calibration; int. internal calibration.