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. 2021 Sep 19;21(18):6287. doi: 10.3390/s21186287

Table 2.

Summary of electrochemical deposition treatment (EDT) processes used in test phases 1, 2 and 3.

Test Phase Specimen No. Pre-Treatment Deposition Post-Treatment Deposition Post-Treatment Baking
Electrolyte Current Duration
TP1 TP1-1 X X X X X X X 60 °C
5 h
TP1-2 0.3 M MgCl2 −2 μA/cm2 24 h X X X
TP1-3 1.0 M MgCl2
TP1-4 3.0 M MgCl2
TP2 TP2-1 X X X X X X X
TP2-2 X X X
TP2-3 2.0 M MgCl2 −2 μA/cm2 48 h
TP2-4 168 h
TP3 TP3-1 X 2.0 M MgCl2 −2 μA/cm2 240 h
(10 days)
NaOH (pH 13) X X
TP3-2 O X
TP3-3 O O
TP3-4 NaOH (pH 13) X X