Skip to main content
. 2021 Apr 8;104(5):1272–1281. doi: 10.1093/jaoacint/qsab052

Table 6.

 Data comparison between the present method and a reported method with real toxic fish (figures are the toxin concentrations in µg/kg)a

Fish Injection Present method
Reported method
CTX1B Epi-deoxyCTX1B DeoxyCTX1B Total CTX1B Epi-deoxyCTX1B DeoxyCTX1B Total
Red snapper 1 0.07 0.04 0.09 0.20 0.12 0.02 0.07 0.21
2 0.06 0.04 0.10 0.20 0.07 0.02 0.03 0.13
3 0.07 0.04 0.08 0.19 0.17 0.04 0.06 0.27
Avg. 0.07 0.04 0.09 0.20 0.12 0.03 0.05 0.20
RSD, % 4.6 2.7 9.0 2.6 32.8 23.6 27.3 27.3
Grouper 1 0.10 0.09 0.20 0.40 0.13 0.05 0.19 0.38
2 0.09 0.08 0.18 0.36 0.10 0.04 0.10 0.23
3 0.12 0.08 0.24 0.43 0.25 0.09 0.27 0.61
Avg. 0.10 0.08 0.21 0.39 0.16 0.06 0.19 0.41
RSD, % 12.0 10.2 13.8 9.8 42.0 37.3 37.1 38.6
White-edged grouper 1 0.04 0.08 0.07 0.19 0.06 0.07 0.08 0.21
2 0.03 0.09 0.07 0.19 0.04 0.05 0.04 0.13
3 0.05 0.07 0.10 0.21 0.12 0.11 0.12 0.35
Avg. 0.04 0.08 0.08 0.19 0.07 0.07 0.08 0.23
RSD, % 20.7 11.9 21.7 7.4 47.4 35.7 39.6 40.6

a Average and RSD, % were calculated from three data points produced from three injections of the same test solution. The NIHS used the reported method (23), whereas JFRL used the present method. The absence of CTX3C and 49-epiCTX3C in fish from Okinawa agrees with the report in the literature (12, 23). The abbreviations are the same as in Figure 9.