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. 2021 May 6;84(5):1587–1597. doi: 10.1021/acs.jnatprod.1c00128

Table 3. 13C NMR Spectroscopic Data for Compounds 1–9.

  1 2 3 4 5 6 7 8 9
position δC, type δC, type δC, type δC, type δC, type δC, type δC, type δC, type δC, type
1 46.5, CH2 46.4, CH2 46.7, CH2 47.6, CH2 47.7, CH2 47.7, CH2 47.6, CH2 47.7, CH2 47.7, CH2
2 68.9, CH 69.0, CH 68.9, CH 69.5, CH 69.5, CH 69.5, CH 69.5, CH 69.5, CH 69.5, CH
3 83.9, CH 84.0, CH 83.9, CH 84.4, CH 84.4, CH 84.4, CH 84.4, CH 84.4, CH 84.4, CH
4 39.3, C 39.3, C 39.3, C 40.5, C 40.5, C 40.5, C 40.5, C 40.5, C 40.5, C
5 55.3, CH 55.3, CH 55.3, CH 56.6, CH 56.6, CH 56.6, CH 56.6, CH 56.6, CH 56.6, CH
6 18.4, CH2 18.4, CH2 18.5, CH2 19.5, CH2 19.5, CH2 19.6, CH2 19.6, CH2 19.5, CH2 19.6, CH2
7 32.4, CH2 32.4, CH2 32.5, CH2 33.7, CH2 33.8, CH2 33.8, CH2 33.7, CH2 33.8, CH2 33.8, CH2
8 39.5, C 39.5, C 39.6, C 40.7, C 40.7, C 40.7, C 40.7, C 40.7, C 40.7, C
9 47.6, CH 47.6, CH 47.7, CH 48.9, CH 49.0, CH 48.9, CH 49.0, CH 49.0, CH 49.0, CH
10 38.3, C 38.3, C 38.4, C 39.2, C 39.2, C 39.2, C 39.2, C 39.2, C 39.2, C
11 23.7, CH2 23.7, CH2 23.8, CH2 23.9, CH2 24.0, CH2 24.0, CH2 24.0, CH2 24.0, CH2 24.0, CH2
12 125.4, CH 125.4, CH 125.4, CH 123.9, CH 123.8, CH 123.7, CH 123.9, CH 123.8, CH 123.7, CH
13 144.7, C 145.2, C 145.5, C 145.2, C 145.5, C 145.5, C 145.3, C 145.5, C 145.5, C
14 42.1, C 42.2, C 42.3, C 42.9, C 43.0, C 43.0, C 42.9, C 43.0, C 43.0, C
15 29.7, CH2 29.5, CH2 29.8, CH2 30.2, CH2 30.4, CH2 30.6, CH2 30.3, CH2 30.5, CH2 30.7, CH2
16 23.7, CH2 23.7, CH2 23.8, CH2 24.6, CH2 24.6, CH2 24.7, CH2 24.7, CH2 24.7, CH2 24.7, CH2
17 46.4, C 46.6, C 46.4, C 47.6, C 47.5, C 47.5, C 47.6, C 47.5, C 47.5, C
18 41.9, CH 42.4, CH 42.6, CH 42.5, CH 42.6, CH 42.6, CH 42.5, CH 42.6, CH 42.7, CH
19 46.8, CH2 46.9, CH2 46.9, CH2 48.1, CH2 48.1, CH2 48.1, CH2 48.1, CH2 48.1, CH2 48.1, CH2
20 30.9, C 30.9, C 30.9, C 31.6, C 31.6, C 31.6, C 31.6, C 31.6, C 31.6, C
21 34.3, CH2 34.2, CH2 34.3, CH2 35.1, CH2 35.1, CH2 35.1, CH2 35.1, CH2 35.1, CH2 35.1, CH2
22 33.0, CH2 32.6, CH2 32.7, CH2 34.4, CH2 34.4, CH2 34.3, CH2 34.4, CH2 34.4, CH2 34.3, CH2
23 28.7, CH3 28.7, CH3 28.8, CH3 29.3, CH3 29.3, CH3 29.3, CH3 29.3, CH3 29.3, CH3 29.3, CH3
24 16.8, CH3 16.9, CH3 16.9, CH3 17.5, CH3 17.5, CH3 17.5, CH3 17.4, CH3 17.5, CH3 17.5, CH3
25 16.8, CH3 16.9, CH3 16.9, CH3 17.1, CH3 17.1, CH3 17.2, CH3 17.1, CH3 17.1, CH3 17.2, CH3
26 17.1, CH3 17.1, CH3 17.2, CH3 17.8, CH3 18.0, CH3 18.1, CH3 17.9, CH3 18.0, CH3 18.1, CH3
27 25.9, CH3 25.9, CH3 25.9, CH3 26.5, CH3 26.5, CH3 26.5, CH3 26.5, CH3 26.4, CH3 26.5, CH3
28 178.3, C 178.4, C 178.1, C 180.4, C 180.2, C 180.1, C 180.5, C 180.3, C 180.2, C
29 23.7, CH3 23.7, CH3 25.9, CH3 24.0, CH3 24.0, CH3 24.0, CH3 24.1, CH3 24.0, CH3 24.0, CH3
30 33.2, CH3 33.1, CH3 33.2, CH3 33.6, CH3 33.6, CH3 33.6, CH3 33.6, CH3 33.5, CH3 33.6, CH3
1′ 37.0, CH2 39.9, CH2 40.2, CH2 37.5, CH2 40.5, CH2 40.7, CH2 37.8, CH2 40.5, CH2 40.8, CH2
2′ 27.5, CH2 29.3, CH2 29.6, CH2 28.5, CH2 28.5, CH2 30.5, CH2 28.5, CH2 28.5, CH2 30.5, CH2
3′ 36.2, CH2 26.9, CH2 29.6, CH2 37.5, CH2 27.6, CH2 28.5, CH2 37.8, CH2 27.8, CH2 28.4, CH2
4′   27.4, CH2 29.6, CH2   27.6, CH2 30.5, CH2   27.8, CH2 30.5, CH2
5′   26.9, CH2 29.6, CH2   30.3, CH2 30.5, CH2   30.4, CH2 30.5, CH2
6′   39.6, CH2 29.6, CH2   40.5, CH2 30.5, CH2   40.5, CH2 30.5, CH2
7′     27.4, CH2     28.1, CH2     28.4, CH2
8′     27.4, CH2     28.1, CH2     28.1, CH2
9′     27.4, CH2     30.5, CH2     30.5, CH2
10′     39.6, CH2     40.7, CH2     40.8, CH2
1″             127.7, C 127.8, C 127.7, C
2″ 161.5, C 161.6, C 161.6, C 163.4, C 163.4, C 163.4, C 130.6, CH 130.5, CH 130.5, CH
3″ 118.4, C 118.6, C 118.7, C 113.2, CH 113.0, CH 113.0, CH 116.8, CH 116.7, CH 116.7, CH
4″ 148.5, CH 148.4, CH 148.4, CH 152.5, C 152.7, C 152.7, C 160.6, C 160.5, C 160.5, C
4a″ 118.7, C 118.8, C 118.8, C 113.1, C 113.1, C 113.1, C      
5″ 129.9, CH 129.9, CH 130.0, CH 127.5, CH 127.5, CH 127.5, CH 116.8, CH 116.7, CH 116.7, CH
6″ 122.7, CH 122.7, CH 122.6, CH 114.4, CH 114.3, CH 114.4, CH 130.6, CH 130.5, CH 130.5, CH
7″ 134.3, CH 134.2, CH 134.1, CH 163.1, C 163.1, C 163.1, C 142.0, CH 141.7, CH 141.7, CH
8″ 116.8, CH 116.7, CH 116.8, CH 103.8, CH 103.7, CH 103.7, CH 118.3, CH 118.5, CH 118.5, CH
8a″ 154.5, C 154.5, C 154.6, C 156.8, C 156.8, C 156.8, C      
9″ 162.2, C 161.6, C 161.7, C 37.8, CH2 40.3, CH2 40.3, CH2 169.4, C 169.2, C 169.2, C
10″       171.0, C 170.7, C 170.7, C