Table 2.
Average recovery percentages ± relative standard deviation (RSD) for 18 OCPs extracted from fortified laboratory blank-liver, -gills, and –muscles tissue samples of fish using QuEChERS technique with two levels of the multi-standards mixture (0.1 and 1 µg/Kg)
OCPs | 0.1 µg/Kg | 1 µg/Kg | ||||
---|---|---|---|---|---|---|
Liver | Gills | Muscles | Liver | Gills | Muscles | |
α-HCH | 93.1 ± 1.3 | 95.1 ± 3.2 | 91.2 ± 6.1 | 94.1 ± 1.3 | 94.1 ± 3.2 | 90.2 ± 6.1 |
γ-HCH | 95.1 ± 1.3 | 96.1 ± 4.2 | 94.2 ± 5.1 | 93.1 ± 1.3 | 94.1 ± 4.2 | 93.2 ± 5.1 |
β-HCH | 96.2 ± 2.3 | 97.3 ± 3.2 | 96.1 ± 6.1 | 97.2 ± 2.3 | 99.3 ± 3.2 | 95.1 ± 6.1 |
Heptachlor | 97.3 ± 4.1 | 98.1 ± 2.2 | 97.1 ± 6.1 | 98.3 ± 4.1 | 96.1 ± 2.2 | 98.1 ± 6.1 |
δ-HCH | 98.3 ± 5.1 | 99.1 ± 3.1 | 99.1 ± 5.1 | 96.3 ± 5.1 | 97.1 ± 3.1 | 97.1 ± 5.1 |
Aldrin | 93.3 ± 2.2 | 98.2 ± 2.2 | 100.1 ± 3.2 | 92.3 ± 2.2 | 95.2 ± 2.2 | 98.1 ± 3.2 |
Heptachlorepoxide | 99.1 ± 3.2 | 99.2 ± 3.2 | 99.1 ± 5.2 | 97.1 ± 2.2 | 98.2 ± 3.2 | 99.1 ± 5.2 |
Endosulfan Ι | 98.1 ± 2.5 | 100.1 ± 1.2 | 100.1 ± 3.2 | 98.1 ± 2.5 | 98.1 ± 1.2 | 97.1 ± 3.2 |
p,p-DDE | 100.1 ± 3.5 | 92.2 ± 3.2 | 99.1 ± 6.1 | 98.1 ± 3.5 | 95.2 ± 3.2 | 98.1 ± 6.1 |
Dieldrin | 98.2 ± 2.5 | 99.1 ± 3.2 | 94.2 ± 3.2 | 96.2 ± 3.5 | 98.1 ± 3.2 | 93.2 ± 3.2 |
Endrin | 93.2 ± 5.1 | 100.2 ± 3.4 | 99.2 ± 4.1 | 93.2 ± 5.1 | 98.2 ± 3.4 | 98.2 ± 4.1 |
p,p-DDD | 94.5 ± 3.2 | 93.2 ± 2.3 | 95.3 ± 5.2 | 95.5 ± 3.2 | 95.2 ± 2.3 | 93.3 ± 5.2 |
Endosulfan Π | 95.6 ± 2.2 | 94.2 ± 2.4 | 91.1 ± 3.2 | 96.6 ± 2.2 | 96.2 ± 2.4 | 96.1 ± 3.2 |
p,p-DDT | 96.7 ± 3.2 | 98.2 ± 3.1 | 99.1 ± 3.3 | 97.7 ± 3.2 | 95.2 ± 3.1 | 98.1 ± 3.3 |
Endrin aldehyde | 99.1 ± 3.1 | 99.1 ± 4.1 | 100.3 ± 2.3 | 98.1 ± 3.1 | 96.1 ± 4.1 | 97.3 ± 2.3 |
Endosulfan sulphate | 98.1 ± 2.5 | 98.2 ± 3.2 | 92.1 ± 4.1 | 96.1 ± 1.5 | 95.2 ± 3.2 | 96.1 ± 4.1 |
Methoxychlor | 99.9 ± 2.3 | 100.1 ± 2.2 | 91.2 ± 3.2 | 97.9 ± 1.3 | 98.1 ± 2.2 | 95.2 ± 3.2 |
Endrin ketone | 98.9 ± 2.5 | 95.6 ± 3.2 | 93.2 ± 3.2 | 96.9 ± 2.5 | 94.6 ± 3.2 | 97.2 ± 3.2 |
n = 3 Replicates