Table 1. Summary of the Mean Particle Dimensiona.
sample | DTEM ± σ (nm) | DXRD-311 ± σ (nm) | Ms at RT (Am2/kg) | Ms at 5 K (Am2/kg) | Hc at RT (mT) | Hc at 5 K (mT) | Mr/Ms at RT | Mr/Ms at 5 K | Keff at 5 K (kJ/m3) | Keff at 300 K (kJ/m3) |
---|---|---|---|---|---|---|---|---|---|---|
A | 23 (2) | 23 (1) | 85 (2) | 96 (2) | 0.9 (2) | 43.6 (2) | 0.1 | 0.49 | 24.0 (5) | 13.5 (5) |
B | 29 (3) | 28 (1) | 90 (2) | 98 (2) | 5.2 (2) | 52.3 (2) | 0.26 | 0.49 | 27.5 (5) | 11.0 (5) |
Obtained by TEM (DTEM), size of the crystalline domain (DXRD) by Scherrer calculation, saturation magnetization (MS) at RT and 5 K, coercivity (Hc) at RT and 5 K, reduced remanence at RT and 5 K and effective anisotropy constant (Keff) obtained from the simulations of DC loops at 5 K and AC loops at 300 K.