| Refinement on F2 | H atoms treated by a mixture of independent and constrained refinement |
| Least-squares matrix: full | w = 1/[σ2(Fo2) + (0.0516P)2 + 0.144P] where P = (Fo2 + 2Fc2)/3 |
| R[F2 > 2σ(F2)] = 0.036 | (Δ/σ)max = 0.001 |
| wR(F2) = 0.098 | Δρmax = 0.17 e Å−3 |
| S = 1.02 | Δρmin = −0.14 e Å−3 |
| 2976 reflections | Extinction correction: SHELXL-2014/7 (Sheldrick, 2015), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
| 242 parameters | Extinction coefficient: 0.0034 (4) |
| 2 restraints | Absolute structure: Flack x determined using 1053 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons et al., 2013) |
| Primary atom site location: structure-invariant direct methods | Absolute structure parameter: 0.2 (2) |
| Hydrogen site location: mixed |