| Refinement on F2 | Hydrogen site location: inferred from neighbouring sites |
| Least-squares matrix: full | H-atom parameters constrained |
| R[F2 > 2σ(F2)] = 0.028 | w = 1/[σ2(Fo2) + (0.0239P)2 + 18.7547P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.065 | (Δ/σ)max = 0.002 |
| S = 1.06 | Δρmax = 1.43 e Å−3 |
| 9046 reflections | Δρmin = −1.83 e Å−3 |
| 427 parameters | Extinction correction: SHELXL-2014/7 (Sheldrick, 2015b), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
| 45 restraints | Extinction coefficient: 0.000167 (12) |
| Primary atom site location: dual |