Skip to main content
. 2021 Oct 7;11:19915. doi: 10.1038/s41598-021-99064-8

Table 1.

Tandem oxidative cyclization of compound 3.

Sr. No. Reaction conditions Time (h) Yield of 1 (%)
1 Ru(bpz)3(PF6)2 (0.1 equiv), (NH4)2S2O8 (2 equiv), CH3CN, Ar, blue LED, r.t 18 Decomposed
2 Acridinium (0.1 equiv), TBHP (2 equiv), CH3CN, Ar, blue LED, r.t 48 Decomposed
3 CAN (2.5 equiv), CH3CN, Ar, 0 °C 2 Decomposed
4 Mn(OAc)3·2H2O (4 equiv), CH3CN, Ar, reflux 5 Decomposed
5 PIFA (1.2 equiv), HFIP, Ar, r.t 4 Decomposed
6a Glassy carbon anode, Glassy carbon cathode, 0.1M LiClO4, 1.25 V 18
7a Platinum anode, Glassy carbon cathode, 0.1MLiClO4,1.25 V 10

aPassivation of electrode observed.