Table 2. HG-MC-ICPMS Operating Parameters.
| MC-ICPMS parameters | |
| RF power | 1300 W |
| coolant flow (Ar) | 13 L/min |
| auxiliary flow (Ar) | 1.15 L/min |
| nebulizer gas flow (Ar) | 0.69 L/min |
| interface cones | nickel |
| measurement parameters | |
| resolution mode | ∼300 |
| cup configuration | H4: 74Ge; H2: 73Ge; Ax: 72Ge; L4: 70Ge |
| integration time | 2.5 s |
| measurement mode | time-resolved analysis |
| replicates | ≥50 |
| hydride generation | |
| “acid” reagent | 0.1 M sodium acetate buffer |
| reducing agent | NaBH4 (1%) mixed with NaOH (0.01 M) |
| reagents and sample flow rate | 0.83 mL/min |
| sample gas rotameter position | 10 mm |
| additional gas flow rate | 0.7 L/min |