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. 2021 Sep 27;6(40):25972–25981. doi: 10.1021/acsomega.1c02804

Table 2. Scope of the Addition of Carboxylic Acids to Ethenesulfonyl Fluoride (ESF)ab.

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a

Reaction condition: a mixture of carboxylic acid (1, 1.0 mmol), ESF (2.0 mmol), CuO (1.0 equiv), and MeCN (0.2 M, 5.0 mL) reacted at 80 °C under an argon atmosphere for 20 h.

b

Isolated yield.

c

The reaction was conducted on a 5 mmol scale (1d, 1.00 g).

d

Additional 5 mol % Ru(bpy)3(PF6)2 was added.