Table 5. Summary of Yields and Properties of (3BS)2-SiPc Samples.
| 3BS | AQ | BG | PR |
|---|---|---|---|
| crude yield | 57% (2.61 g) | 81% (1.69 g) | ≪50% (0.86 g) |
| sublimation yield | 91% (0.29 g) | 59% (0.2 g) | 48% (0.139 g) |
| Td, 5% | 293 °C | 281 °C | 289 °C |
| Tm,1/Tm,2 | 63 °C/234 °C | 63 °C/234 °C | 63 °C/234 °C |
| ΔHm,1/ΔHm,2 (J/g) | 29.7/40.4 | 35.4/23.7 | 38.6/38.6 |
| Tc,1/Tc,2 | 63 °C/212 °C | 61 °C/200 °C | 62 °C/196 °C |
| ΔHc,1/ΔHc,2 (J/g) | 25.6/44.2 | 33.5/38.6 | 33.9/39.4 |