Table 13.
Scope of aryl iodides.a.
|
Standard conditions are 4e (0.2 mmol, 1.0 equiv), 2 (2.0 equiv), Pd(OAc)2 (10 mol %), L2 (20 mol %), N9 (30 mol %), AgOAc (2.0 equiv), CHCl3 (1.0 mL, 0.2 M), under air, 100 °C, 12 hours.
110 °C.
24 hours.
Scope of aryl iodides.a.
|
Standard conditions are 4e (0.2 mmol, 1.0 equiv), 2 (2.0 equiv), Pd(OAc)2 (10 mol %), L2 (20 mol %), N9 (30 mol %), AgOAc (2.0 equiv), CHCl3 (1.0 mL, 0.2 M), under air, 100 °C, 12 hours.
110 °C.
24 hours.