Table 1.
Element Isotope | Instrument Mode | Cell Gas | Quantitated Ion | Quantitated Mass | Internal Standard |
---|---|---|---|---|---|
27Al | MS-MS | H2 | 27Al+ | 27 | 169Tm+ |
52Cr | MS-MS | NH3 | 52Cr(NH3)2+ | 86 | 103Rh(NH3)4+ |
56Fe | MS-MS | NH3 | 56Fe(NH3)2+ | 90 | 103Rh(NH3)4+ |
59Co | MS-MS | NH3 | 59Co(NH3)2+ | 93 | 103Rh(NH3)4+ |
60Ni | MS-MS | O2 | 60NiO+ | 76 | 103RhO+ |
63Cu | MS-MS | NH3 | 63Cu(NH3)2+ | 97 | 103Rh(NH3)4+ |
111Cd | MS-MS | O2 | 111Cd+ | 111 | 103RhO+ |
118Sn | SQ | No Gas | 118Sn+ | 118 | 103Rh+ |
137Ba | SQ | No Gas | 137Ba+ | 137 | 169Tm+ |
206+207+208Pb | SQ | No Gas | 206+207+208Pb+ | 206 + 207 + 208 | 103Rh+ |
Cell parameters: 0.55 mL/min O2 cell gas with −20 V octopole bias, −8 V energy discrimination;.4.5 mL/min 10% NH3, 90% He cell gas with −18 V octopole bias, −8 V energy discrimination. 5.0 mL/min H2 cell gas with −18 V octopole bias, 0 V energy discrimination; No Gas with −8 V octopole bias, 5 V energy discrimination. SQ: Single Quad mode, MS-MS: triple quad mode.