Table 2. Results of Accuracy and Intraday/Interday Precision for Three Concentration Levels Using the GC-MS Methoda (Revised).
| day 1 |
day 2 |
day 3 |
|||||||
|---|---|---|---|---|---|---|---|---|---|
| accuracy | precision |
accuracy | precision |
accuracy | precision |
||||
| concentration (μg/mL) | (%recovery) | SD | RSD (%) | (%recovery) | SD | RSD (%) | (%recovery) | SD | RSD (%) |
| 5 | 100.30 | 1.17 | 1.16 | 100.62 | 0.79 | 0.79 | 101.44 | 0.37 | 0.36 |
| 10 | 100.90 | 0.74 | 0.73 | 100.73 | 0.96 | 0.95 | 100.81 | 0.20 | 0.20 |
| 15 | 100.19 | 0.16 | 0.16 | 100.10 | 0.05 | 0.05 | 100.69 | 0.09 | 0.09 |
| confidence interval (%) | 98.98–101.74 | 99.64–101.81 | 99.59–101.85 | ||||||
Acceptance criteria: %Recovery: 95–105%; RSD: 3.7% SD = standard deviation. RSD = relative standard deviation.