Figure 2.

(A) Synthesis of key macrolactone 21. (B) Partial HMBC data for 21; key correlations between H11 → C16 and H15a/b → C12.

(A) Synthesis of key macrolactone 21. (B) Partial HMBC data for 21; key correlations between H11 → C16 and H15a/b → C12.