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. Author manuscript; available in PMC: 2022 Jul 16.
Published in final edited form as: ACS Catal. 2021 Jun 30;11(14):8585–8590. doi: 10.1021/acscatal.1c02406

Scheme 3. Mechanistic investigation.

Scheme 3.

aStandard conditions: [Cp*RhCl2]2 (5 mol%), NaHCO3 (30 mol%), MeOH (0.6 M), dioxazolone (1 equiv), arylboronic acid (2.5 equiv), alkene (3 equiv), 25 °C. b1) 6 M HCl; 2) SOCl2, MeOH; 3) Picolinic acid, EDCI, HOBt, DCM; 4) Pd(OAc)2, PhI(OAc)2, DCM.