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. Author manuscript; available in PMC: 2021 Nov 8.
Published in final edited form as: J Nat Prod. 2021 May 6;84(5):1656–1665. doi: 10.1021/acs.jnatprod.1c00248

Table 4.

13C NMR spectral data of berkeleypenostatins 2–7 in MeOH-d4 (100 MHz)

2 3 4 5 6 7
carbon δC, type δC, type δC, type δC, type δC, type δC, type
1 203.7, C 203.2, C 83.5, C 195.5, C 195.4, C 198.7, C
2 46.7, CH2 46.6, CH2 125.2, C 120.7, CH 120.7, CH 121.4, CH
3 91.8, C 90.4, C 147.9, C 176.8, C 175.3, C 175.0, C
4 45.4, CH2 42.5, CH2 39.0, CH2 41.6, CH2 41.3, CH2 41.2, CH2
5 73.1, CH 78.2, CH 80.8, CH 79.4, CH 78.9, CH 79.1, CH
6 42.1, CH2 39.2, CH2 41.0, CH2 37.5, CH2 37.0, CH2 36.7, CH2
7 49.6, CH 50.0, CH 50.1, CH 47.8, CH 47.5, CH 46.4, CH
8 41.2, CH 41.5, CH 51.8, CH 46.7, CH 46.8, CH 46.5, CH
9 84.4, C 84.5, C 213.4, C 92.8, C 92.9, C 75.3, CH
10 121.3, CH 121.3, CH 128.8, CH 121.4, CH 121.4, CH 123.4, CH
11 137.6, C 137.6, C 131.2, C 135.4, C 135.6, C 137.2, C
12 80.8, CH 80.8, CH 131.5, CH 77.8, CH 77.7, CH 79.1, CH
13 131.2, CH 131.1, CH 134.4, CH 129.7, CH 129.6, CH 127.8, CH
14 137.2, CH 137.3, CH 44.9, CH 137.4, CH 137.2, CH 137.5, CH
15 33.2, CH2 33.5, CH2 29.3, CH2 33.4, CH2 33.4, CH2 33.5, CH2
16 30.3, CH2 30.3, CH2 28.0, CH2 30.5, CH2 30.4, CH2 30.4, CH2
17 30.4, CH2 30.4, CH2 29.5, CH2 30.4, CH2 30.3, CH2 30.3, CH2
18 30.6, CH2 30.4, CH2 29.2, CH2 30.4, CH2 30.3, CH2 30.3, CH2
19 33.3, CH2 33.2, CH2 30.9, CH2 33.2, CH2 33.2, CH2 33.2, CH2
20 23.9, CH2 23.8, CH2 28.3, CH2 23.8, CH2 23.8, CH2 23.8, CH2
21 14.6, CH3 14.6, CH3 14.6, CH3 14.6, CH3 14.6, CH3 14.6, CH3
22 20.4, CH3 20.2, CH3 25.8, CH3 19.8, CH3 19.7, CH3 20.2, CH3
23 170.9, C 171.0, C
1’ 104.2, CH 103.4, CH 103.6, CH 103.6, CH 103.1, CH
2’ 75.2, CH 75.1, CH 75.1, CH 75.2, CH 75.2, CH
3’ 80.0, CH 78.2, CH 78.1, CH 78.2, CH 78.2, CH
4’ 71.7, CH 71.8, CH 71.8, CH 71.8, CH 71.8, CH
5’ 78.2, CH 75.1, CH 78.1, CH 79.0, CH 78.2, CH
6’ 63.0, CH2 62.9, CH2 62.9, CH2 63.0, CH2 62.9, CH2