. 2021 Sep 23;86(21):14508–14552. doi: 10.1021/acs.joc.1c01376

Table 1. 1,5-HAT–S–T Sequence in 3-C-(α,β-d-Glcp)1-propoxyphthalimides 1–4^a.

Reagents and conditions: method A: n-Bu₃SnH (1 equiv), AIBN (0.1 equiv), PhCH₃ (0.013 M), reflux; method B: n-Bu₃SnH (1 equiv/h), AIBN (0.1 equiv), PhCH₃ (0.013 M), reflux; method C: TTMSS (1 equiv), AIBN (0.1 equiv), PhCH₃ (0.013 M), reflux; and method D: n-Bu₃SnD (1 equiv), AIBN (0.1 equiv), PhCH₃ (0.013 M), reflux.

Values in parentheses are isolate yields; deuterium incorporation (²H/¹H) is included in partially labeled compounds.

Table 1. 1,5-HAT–S–T Sequence in 3-C-(α,β-d-Glcp)1-propoxyphthalimides 1–4a.

Table 1. 1,5-HAT–S–T Sequence in 3-C-(α,β-d-Glcp)1-propoxyphthalimides 1–4^a.