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. Author manuscript; available in PMC: 2021 Nov 10.
Published in final edited form as: Front Environ Sci. 2021 Feb 16;8:575614. doi: 10.3389/fenvs.2020.575614

TABLE 6 |.

Effects of microplastics in oxidative stress and membrane integrity.

End-point Polymer type Exposure time Size Concentration range Assay Cell type Outcome Ref

Oxidative stress Polystyrene (PS) and arsenic (As) 12 h 0.1 and 5 um 20 ug/ml (0.1 um), 80 ug/ml (0.5 um) As:75 and 150 ug/l DCFH-DA kit assay Caco-2 cells ROS increased after the co-exposure (PS + As), comparing to just arsenic exposure Wu et al. (2019)
Polystyrene (PS) 12 h 0.1 and 5 um 1–200 ug/ml DCFH-DA kit assay Caco-2 cells ROS production only increased after 200 ug/ml exposure to 0.1 um and 5 um PS. Wu et al. (2019)
24 h 1.72 ± 0.26 um 10–1000 ug/cm2 Western blot (HO-1) DCFH-DA kit assay BEAS-2B cells HO-1 protein level significantly increased after 10 and 1000 ug/cm2 DCFH-DA increased at 1000 ug/cm2 Dong et al. (2020)
10 um 0.05–10 mg/L DHE solution T98G and HeLa cells ROS increased in both cell lines. EC50 9.6 mg/L in T98G and EC50 13.56 mg/L in HeLa cells Schirinz et al. (2017)
24 h, 48 h 5 um 12.5–50 mg/L SOD, GSH, MDA detection and CAT activity Caco-2 cells No effect on SOD, GSH and MDA levels. Activity of catalase was inhibited only after 24 and 48 h exposure to 50 mg/L of 5 um PS Wu et al (2020).
Polyethylene (PE) 24 h 3–16 um 0.05–10 mg/L DHE solution T98G and HeLa cells ROS increased only in T98G cells. EC50 41.22 mg/L Schirinzi et al. (2017)
Polypropylene (PP) 6 h 20 and 25–200 um 50–1,000 ug/ml in powder and DMSO DCFH-DA kit assay HDF cells ROS increased after exposure to 20 um PP (in DMSO) at 1000 ug/mL. When administered in powder, ROS did not increase Hwan et al. (2019)
Membrane integrity Polystyrene (PS) 12 h 0.1 and 5 um 1–80 ug/mL JC1 assay, LDH assay and TMA-DPH Caco-2 cells Mitochondrial membrane depolarization occurred after 20 to 80 ug/mL for 0.1 um PS and after all the concentrations of 5 um. No effects on LDH leakage or polarization Wu et al. (2019)
24 h 1.72 ± 0.26 um 10–1000 ug/cm2 TEER, ELISA (ZO-1 and AAT) and Western blot (ZO-1) BEAS-2B cells TEER value decreased in the epithelial barrier after 10 and 1,000 ug/cm2 exposure. ZO-1 levels decreased after exposure to 10 and 1000 ug/cm2. AAT level decreased after exposure to 1,000 ug/cm2 Dong et al. (2020)
COOH-modified polystyrene (PS) 24 h 5 um 10–100 μg/ml TEER GIT barrier and placental barrier coculture model No effect in GIT or placental barrier were observed Hesler et al. (2019)
Immune response Polystyrene (PS) 24 h 1.72 ± 0.26 um 10–1000 ug/cm2 ELISA (IL-6, IL-8) BEAS-2B cells IL-6 significantly increased at 10 and 1000 ug/cm2 exposure. 1000 ug/cm2 exposure increased IL-8 expression Dong et al. (2020)
24 h, 48 h 5 um 12.5–50 mg/L RT-PCR Caco-2 cells Four inflammation related genes (TRPV1, iNOS, IL-1β, IL-8) were up-regulated Wu et al. (2020)
24 h, 72 h 1, 4 and 10 um 100,000/ml (1 um), 250,000/ml (4 um), 60,000/ml (10 um) Macrophage polarization (Western Blot and RT-PCR) THP-1 cells No macrophage differentiation Stock et al. (2019)
Polypropylene (PP) 4 h, 72 h, 4 days 20 and 25–200 um 10–1,000 ug/ml ELISA (IL-2, IL-6, IL-10, TNF-α) PBMC PBMC: IL-6 increased after 20 um PP at 1,000 and 100 ug/ml and TNF-α increased after 100 ug/mL after 20 um size exposure Hwang et al.,(2019)
48 h 20 and 25–200 um 100 ug/ml and 500 ug/ml (20 um and 25–200 um) Histamine by ELISA kit HMC-1 cells Histamine was released after exposure to 500 ug/ml 20 um PP in HMC-1 cells Hwang et al.,(2019)

Abbreviations: PS, Polystyrene; PE, Polyethylene; PP, Polypropylene.