TABLE 1.
Atomic ratio |
||||
---|---|---|---|---|
Inclusion | Mg Kα | P Kα | Ca Kα | Ca/P ratio |
Type II inclusion 1 | 4.92 | 31.38 | 63.7 | 2.03 |
Type II inclusion 2 | 2.41 | 33.92 | 63.67 | 1.88 |
Type II inclusion 3 | 0.84 | 38.37 | 60.79 | 1.58 |
Type II inclusion 4 | 0 | 31.59 | 68.41 | 2.17 |
Type II inclusion 5 | 5.65 | 40.11 | 54.24 | 1.35 |
Type II inclusion 6 | 0 | 23.08 | 76.92 | 3.33 |
Type II inclusion 7 | 2.03 | 30.56 | 67.41 | 2.21 |
Type II inclusion 8 | 9.78 | 55.75 | 34.47 | 0.62 |
Type II inclusion 9 | 2.01 | 21.09 | 76.9 | 3.64 |
Type II inclusion 10 | 0 | 51.38 | 48.62 | 0.95 |
Avg | 2.76 | 35.73 | 61.51 | 1.72 |
Polyphosphate 1 | 14.63 | 68.73 | 16.64 | 0.24 |
Polyphosphate 2 | 14.28 | 67.93 | 17.79 | 0.26 |
Polyphosphate 3 | 19.31 | 64.30 | 16.39 | 0.25 |
Polyphosphate 4 | 18.91 | 64.99 | 16.10 | 0.25 |
Polyphosphate 5 | 17.87 | 65.20 | 16.93 | 0.26 |
Polyphosphate 6 | 16.34 | 66.79 | 16.87 | 0.25 |
Polyphosphate 7 | 17.49 | 67.46 | 15.05 | 0.22 |
Polyphosphate 8 | 16.31 | 66.91 | 16.78 | 0.25 |
Avg | 16.9 | 66.5 | 16.6 | 0.25 |
See reference 30. Positions of type II inclusions on STEM-HAADF images are shown in Fig. S5 in the supplemental material. Kα, the X ray is emitted when vacancy in K-shell is filled by a transition from L-shell.