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. 2021 Oct 25;14(21):6401. doi: 10.3390/ma14216401

Table 3.

Chemical recycling methods.

Chemical Agents Reaction Conditions Tensile Strength Retention Ref.
Nearcritical and supercritical water 250–400 °C, 4–27 MPa, 1–30 min 90–98% [81]
Water + benzyl alcohol 400 °C, 1 h [79]
NaCl 1 dissolution Electrochemical (4–25 mA) 80% [46]
Hydrochloric acid in tetrahydrofuran Room temp., 24 h Similar to virgin fibers [82]
AlCl3 2 + Acetic acid 180 °C, 6 h 97.77% [83]
Ethylene glycol 180 °C, 4 h 95% [84]
Supercritical 1-propanol with 1% KOH 3 330 °C, 1 h 94.6% [85]
Sub- and supercritical water and water/ethanol (50:50) 350–400 °C, 25 MPa Similar to desized virgin fibers [86]
ZnCl2/KOH/HPW 4/MgCl2 5/AlCl3/FeCl3 6 + ethanol/water 80–250 °C, 2–10 h [87]
Water/acetone (20:80) 320 °C, 60 min >90% [88]
Supercritical n-butanol 360 °C, 1 h 98.63% [89]
Supercritical acetone 320 °C, 20 min Negligible decrease [90]
Subcritical water
Supercritical water
400 °C, 15 min
280 °C, 30 min
>90% [91]
Peracetic acid (acetic acid + H2O2 7) 65 °C, 4 h Similar to virgin fibers [48]
Nearcritical water and supercritical acetone 260–300 °C, 6–30 MPa Similar to virgin fibers [92]
Superheated and supercritical acetone 350 °C, 2–14 MPa, 60 min [93]
Benzyltrimethylammonium bromide (BTAB) and sodium dodecyl sulfate (SDS) Process: 100 °C, 1 hDry: 100 °C, 24 h 96.9% [94]

1 Sodium chloride; 2 Aluminium chloride; 3 Potassium hydroxide; 4 Phosphotungstic acid; 5 Magnesium chloride; 6 Ferric chloride; 7 Hydrogen peroxide.