Table 2.
Sample | Tentative Identification | Elemental Formula Compound | Ion | m/z Experimental | m/z Theoretical | Tentative Error ppm |
---|---|---|---|---|---|---|
Leaching Crude Extract | Quercetin-3-D-Galactoside | C21H20O12 | [M-H]− | 463.1211 | 463.1211 * | 0 |
Malvidin-3-Glucoside | C23H25O12 | [M+H]+ | 331.0715 | 331.0641 * | −22.3 | |
Delphinidin 3-Glucoside | C21H20O12 | [M+H]+ | 303.0402 | 303.0402 * | 0 | |
Cyanidin 3-Glucoside | C21H21O11+ | [M-H]− | 447.1285 | 447.1242 * | −9.61 | |
Petunidin-3-O-β-Glucoside | C22H23O12 | [M-H]− | 447.1285 | 447.1033 | - | |
Gallic acid | C7H6O5 | [M-H]− | 169.0686 | 169.0606 | - | |
Sinapic acid | C11H12O5 | [M-H]− | 223.0993 | 223.0607 | - | |
Genistein | C15H10O5 | [M-H]− | 269.021 | 269.0455 | - | |
Protocatechuic acid | C7H6O4 | [M-H]− | 153.0649 | 153.0188 | - | |
Rutin | C27H30O16 | [M-H]− | 609.1525 | 609.1461 | - | |
Naringenin | C15H12O5 | [M-H]− | 271.0737 | 271.0612 | - | |
Catechin | C15H14O6 | [M-H]− | 289.1219 | 289.0712 | - | |
Glycitein | C16H12O5 | [M+H]+ | 285.0356 | 285.0749 | - | |
Myricetin | C15H10O8 | [M-H]− | 317.0705 | 317.0303 | - | |
Ferulic acid | C10H10O4 | [M-H]− | 193.0635 | 193.0506 | - | |
Daidzin | C21H20O9 | [M-H]− | 415.09 | 415.1 | - | |
p-coumaric acid | C9H8O3 | [M-H]− | 163.1649 | 163.0395 | - | |
Caffeic acid | C15H10O4 | [M-H]− | 179.1075 | 179.0345 | - | |
Rosmarinic acid | C18H16O8 | [M-H]− | 359.1975 | 359.0767 | - | |
Leaching Pure Extract | Quercetin-3-D-Galactoside | C21H20O12 | [M-H]− | 463.1255 | 463.1211 * | −9.5 |
Malvidin-3-Glucoside | C23H25O12 | [M+H]+ | 331.0715 | 331.0641 * | −22.3 | |
Delphinidin 3-Glucoside | C21H20O12 | [M+H]+ | 303.0438 | 303.0402 * | −11.8 | |
Cyanidin 3-Glucoside | C21H21O11+ | [M-H]− | 447.1328 | 447.1242 * | −9.61 | |
Petunidin-3-O- β -Glucoside | C22H23O12 | [M-H]− | 447.1422 | 447.1033 | - | |
Gallic acid | C7H6O5 | [M-H]− | 169.0713 | 169.0606 | - | |
Protocatechuic acid | C7H6O4 | [M-H]− | 153.07 | 153.0188 | - | |
Rutin | C27H30O16 | [M-H]− | 609.1423 | 609.1461 | - | |
Naringenin | C15H12O5 | [M-H]− | 271.0737 | 271.0612 | - | |
Rosmarinic acid | C18H16O8 | [M-H]− | 359.2091 | 359.0767 | - | |
Catechin | C15H14O6 | [M-H]− | 289.1184 | 289.0712 | - | |
Glycitein | C16H12O5 | [M+H]+ | 285.0356 | 285.0749 | - | |
Myricetin | C15H10O8 | [M-H]− | 317.0823 | 317.0303 | - | |
Ferulic acid | C10H10O4 | [M-H]− | 193.1005 | 193.0506 | - | |
SFE Crude Extract | Quercetin-3-D-Galactoside | C21H20O12 | [M-H]− | 463.0462 | 463.0876 * | 89.4 |
Cyanidin 3-Glucoside | C21H21O11+ | [M-H]− | 447.0592 | 447.1242 * | 145.3 | |
Gallic acid | C7H6O5 | [M-H]− | 169.0207 | 169.0606 | - | |
Caffeic acid | C15H10O4 | [M-H]− | 179.0829 | 179.0345 | - | |
Daidzin | C21H20O9 | [M-H]− | 415.0513 | 415.1 | - | |
Sinapic acid | C11H12O5 | [M-H]− | 223.0014 | 223.0607 | - | |
Naringenin | C15H12O5 | [M-H]− | 271.0333 | 271.0612 | - | |
Rosmarinic acid | C18H16O8 | [M-H]− | 359.1432 | 359.0767 | - | |
Catechin | C15H14O6 | [M-H]− | 289.0766 | 289.0712 | - | |
Myricetin | C15H10O8 | [M-H]− | 317.0568 | 317.0303 | - | |
Ferulic acid | C10H10O4 | [M-H]− | 193.0436 | 193.0506 | - | |
SFE Pure Extract | Quercetin-3-D-Galactoside | C21H20O12 | [M-H]− | 463.0462 | 463.0872 * | 89.4 |
Cyanidin 3-Glucoside | C21H21O11+ | [M-H]− | 447.0679 | 447.1242 * | 125.9 | |
Gallic acid | C7H6O5 | [M-H]− | 169.0367 | 169.0606 | - | |
Caffeic acid | C15H10O4 | [M-H]− | 179.0801 | 179.0345 | - | |
Daidzin | C21H20O9 | [M-H]− | 415.06 | 415.1 | - | |
Sinapic acid | C11H12O5 | [M-H]− | 223.0443 | 223.0607 | - | |
Naringenin | C15H12O5 | [M-H]− | 271.0333 | 271.0612 | - | |
Rosmarinic acid | C18H16O8 | [M-H]− | 359.1432 | 359.0767 | - | |
Catechin | C15H14O6 | [M-H]− | 289.0662 | 289.0712 | - | |
Myricetin | C15H10O8 | [M-H]− | 317.0239 | 317.0303 | - | |
Ferulic acid | C10H10O4 | [M-H]− | 193.0721 | 193.0506 | - |
SFE: Supercritical fluid extraction, * symbol indicates the theoretical m/z obtained with pure standards, while theoretical m/z without the symbol was obtained from MoNa-Mass Bank of North America (https://mona.fiehnlab.ucdavis.edu/) (accessed on 7 July 2021), tentative error ppm was calculated only for the compounds identified with pure standards.