Table 5.
Analytes | Original (μg) |
Spiked (μg) |
Found (μg) |
Recovery (%) |
RSD (%) |
---|---|---|---|---|---|
gallic acid | 29.34 | 20.00 | 45.81 | 99.8 | 1.8 |
40.00 | 68.85 | 97.0 | 1.4 | ||
60.00 | 89.14 | 99.8 | 1.0 | ||
coumalic acid | 9.724 | 6.030 | 14.65 | 87.8 | 4.1 |
12.06 | 21.19 | 95.1 | 2.2 | ||
18.09 | 26.77 | 86.7 | 3.1 | ||
protocatechuic acid | 3.298 | 1.005 | 3.720 | 83.4 | 4.3 |
2.010 | 4.864 | 90.6 | 2.5 | ||
3.015 | 6.338 | 98.4 | 1.4 | ||
proanthocyanidin B1 | 9.027 | 6.000 | 14.01 | 89.7 | 4.0 |
12.00 | 21.58 | 103.6 | 2.3 | ||
18.00 | 26.27 | 94.1 | 2.1 | ||
catechin | 11.43 | 3.000 | 14.15 | 97.7 | 3.6 |
6.000 | 17.50 | 100.1 | 0.7 | ||
9.000 | 20.61 | 100.0 | 0.3 | ||
caffeic acid | 6.539 | 2.972 | 9.33 | 96.3 | 3.4 |
5.945 | 13.14 | 105.0 | 2.1 | ||
8.918 | 15.26 | 98.9 | 1.0 | ||
syringic acid | 6.204 | 2.973 | 8.97 | 97.7 | 3.4 |
5.945 | 12.08 | 97.5 | 3.2 | ||
8.918 | 14.95 | 101.7 | 1.8 | ||
epicatechin | 3.922 | 3030 | 6.932 | 101.2 | 1.6 |
6.060 | 10.04 | 101.9 | 0.7 | ||
9.090 | 13.18 | 105.9 | 1.4 | ||
p-coumaric acid | 4.473 | 3.015 | 7.590 | 105.6 | 3.6 |
6.030 | 10.15 | 92.5 | 1.1 | ||
9.045 | 13.78 | 100.6 | 0.6 | ||
isoquercitrin | 8.802 | 4.040 | 12.75 | 98.1 | 3.2 |
8.080 | 16.75 | 98.8 | 2.1 | ||
12.12 | 20.64 | 98.8 | 1.9 | ||
isorhamnetin-3-O-glucoside | 3.144 | 0.9900 | 4.053 | 98.1 | 1.1 |
1.980 | 5.123 | 97.4 | 2.6 | ||
2.970 | 6.019 | 102.1 | 2.4 | ||
quercetin | 3.146 | 1.966 | 4.928 | 95.5 | 1.6 |
3.933 | 6.950 | 96.7 | 1.3 | ||
5.899 | 8.82 | 92.2 | 4.1 |