| Refinement on F2 | Primary atom site location: structure-invariant direct methods |
| Least-squares matrix: full | Secondary atom site location: difference Fourier map |
| R[F2 > 2σ(F2)] = 0.044 | Hydrogen site location: mixed |
| wR(F2) = 0.129 | H atoms treated by a mixture of independent and constrained refinement |
| S = 1.03 | w = 1/[σ2(Fo2) + (0.0593P)2 + 0.1428P] where P = (Fo2 + 2Fc2)/3 |
| 2774 reflections | (Δ/σ)max < 0.001 |
| 206 parameters | Δρmax = 0.28 e Å−3 |
| 2 restraints | Δρmin = −0.15 e Å−3 |
| 0 constraints |