Br1—C23 | 1.8954 (19) | C12—H12A | 0.9700 |
C1—C8 | 1.344 (3) | C12—H12B | 0.9700 |
C1—O1 | 1.378 (2) | C13—C16 | 1.530 (3) |
C1—C2 | 1.489 (3) | C13—C14 | 1.535 (3) |
C2—C3 | 1.537 (3) | C13—C15 | 1.536 (3) |
C2—H2A | 0.9700 | C14—H14A | 0.9600 |
C2—H2B | 0.9700 | C14—H14B | 0.9600 |
C3—C5 | 1.529 (3) | C14—H14C | 0.9600 |
C3—C4 | 1.530 (3) | C15—H15A | 0.9600 |
C3—C6 | 1.534 (3) | C15—H15B | 0.9600 |
C4—H4A | 0.9600 | C15—H15C | 0.9600 |
C4—H4B | 0.9600 | C16—C17 | 1.489 (3) |
C4—H4C | 0.9600 | C16—H16A | 0.9700 |
C5—H5A | 0.9600 | C16—H16B | 0.9700 |
C5—H5B | 0.9600 | C17—O1 | 1.378 (2) |
C5—H5C | 0.9600 | C18—C24 | 1.380 (3) |
C6—C7 | 1.494 (3) | C18—C19 | 1.395 (2) |
C6—H6A | 0.9700 | C19—C20 | 1.383 (3) |
C6—H6B | 0.9700 | C19—H19 | 0.9300 |
C7—O2 | 1.227 (2) | C20—O5 | 1.378 (2) |
C7—C8 | 1.471 (3) | C20—C22 | 1.400 (3) |
C8—C9 | 1.511 (3) | C21—O5 | 1.403 (3) |
C9—C10 | 1.515 (3) | C21—H21A | 0.9600 |
C9—C18 | 1.530 (2) | C21—H21B | 0.9600 |
C9—H9 | 0.98 (2) | C21—H21C | 0.9600 |
C10—C17 | 1.336 (3) | C22—O4 | 1.362 (2) |
C10—C11 | 1.470 (3) | C22—C23 | 1.384 (3) |
C11—O3 | 1.216 (3) | C23—C24 | 1.387 (3) |
C11—C12 | 1.510 (3) | C24—H24 | 0.9300 |
C12—C13 | 1.533 (3) | O4—H4 | 0.8200 |
C8—C1—O1 | 122.25 (17) | H12A—C12—H12B | 107.6 |
C8—C1—C2 | 126.24 (17) | C16—C13—C12 | 107.75 (17) |
O1—C1—C2 | 111.51 (15) | C16—C13—C14 | 110.89 (18) |
C1—C2—C3 | 112.21 (16) | C12—C13—C14 | 110.14 (19) |
C1—C2—H2A | 109.2 | C16—C13—C15 | 108.20 (18) |
C3—C2—H2A | 109.2 | C12—C13—C15 | 110.44 (19) |
C1—C2—H2B | 109.2 | C14—C13—C15 | 109.39 (19) |
C3—C2—H2B | 109.2 | C13—C14—H14A | 109.5 |
H2A—C2—H2B | 107.9 | C13—C14—H14B | 109.5 |
C5—C3—C4 | 109.3 (2) | H14A—C14—H14B | 109.5 |
C5—C3—C6 | 111.04 (18) | C13—C14—H14C | 109.5 |
C4—C3—C6 | 109.72 (19) | H14A—C14—H14C | 109.5 |
C5—C3—C2 | 109.94 (19) | H14B—C14—H14C | 109.5 |
C4—C3—C2 | 109.43 (17) | C13—C15—H15A | 109.5 |
C6—C3—C2 | 107.36 (18) | C13—C15—H15B | 109.5 |
C3—C4—H4A | 109.5 | H15A—C15—H15B | 109.5 |
C3—C4—H4B | 109.5 | C13—C15—H15C | 109.5 |
H4A—C4—H4B | 109.5 | H15A—C15—H15C | 109.5 |
C3—C4—H4C | 109.5 | H15B—C15—H15C | 109.5 |
H4A—C4—H4C | 109.5 | C17—C16—C13 | 112.68 (16) |
H4B—C4—H4C | 109.5 | C17—C16—H16A | 109.1 |
C3—C5—H5A | 109.5 | C13—C16—H16A | 109.1 |
C3—C5—H5B | 109.5 | C17—C16—H16B | 109.1 |
H5A—C5—H5B | 109.5 | C13—C16—H16B | 109.1 |
C3—C5—H5C | 109.5 | H16A—C16—H16B | 107.8 |
H5A—C5—H5C | 109.5 | C10—C17—O1 | 123.42 (16) |
H5B—C5—H5C | 109.5 | C10—C17—C16 | 125.17 (18) |
C7—C6—C3 | 115.04 (17) | O1—C17—C16 | 111.41 (15) |
C7—C6—H6A | 108.5 | C24—C18—C19 | 119.37 (17) |
C3—C6—H6A | 108.5 | C24—C18—C9 | 119.97 (16) |
C7—C6—H6B | 108.5 | C19—C18—C9 | 120.58 (16) |
C3—C6—H6B | 108.5 | C20—C19—C18 | 120.33 (17) |
H6A—C6—H6B | 107.5 | C20—C19—H19 | 119.8 |
O2—C7—C8 | 119.91 (19) | C18—C19—H19 | 119.8 |
O2—C7—C6 | 121.64 (18) | O5—C20—C19 | 124.98 (18) |
C8—C7—C6 | 118.42 (17) | O5—C20—C22 | 114.18 (16) |
C1—C8—C7 | 117.75 (18) | C19—C20—C22 | 120.84 (17) |
C1—C8—C9 | 123.31 (16) | O5—C21—H21A | 109.5 |
C7—C8—C9 | 118.90 (16) | O5—C21—H21B | 109.5 |
C8—C9—C10 | 109.09 (15) | H21A—C21—H21B | 109.5 |
C8—C9—C18 | 110.02 (15) | O5—C21—H21C | 109.5 |
C10—C9—C18 | 111.38 (15) | H21A—C21—H21C | 109.5 |
C8—C9—H9 | 107.8 (12) | H21B—C21—H21C | 109.5 |
C10—C9—H9 | 110.4 (11) | O4—C22—C23 | 119.68 (17) |
C18—C9—H9 | 108.0 (12) | O4—C22—C20 | 122.66 (17) |
C17—C10—C11 | 118.59 (17) | C23—C22—C20 | 117.67 (16) |
C17—C10—C9 | 122.45 (17) | C22—C23—C24 | 121.99 (17) |
C11—C10—C9 | 118.96 (16) | C22—C23—Br1 | 119.16 (14) |
O3—C11—C10 | 120.3 (2) | C24—C23—Br1 | 118.84 (14) |
O3—C11—C12 | 121.2 (2) | C18—C24—C23 | 119.71 (16) |
C10—C11—C12 | 118.47 (18) | C18—C24—H24 | 120.1 |
C11—C12—C13 | 114.73 (18) | C23—C24—H24 | 120.1 |
C11—C12—H12A | 108.6 | C1—O1—C17 | 118.39 (14) |
C13—C12—H12A | 108.6 | C22—O4—H4 | 109.5 |
C11—C12—H12B | 108.6 | C20—O5—C21 | 117.51 (16) |
C13—C12—H12B | 108.6 | ||
C8—C1—C2—C3 | 24.0 (3) | C12—C13—C16—C17 | 49.6 (2) |
O1—C1—C2—C3 | −156.46 (16) | C14—C13—C16—C17 | −71.0 (2) |
C1—C2—C3—C5 | 72.5 (2) | C15—C13—C16—C17 | 169.04 (18) |
C1—C2—C3—C4 | −167.4 (2) | C11—C10—C17—O1 | 175.94 (16) |
C1—C2—C3—C6 | −48.4 (2) | C9—C10—C17—O1 | −4.1 (3) |
C5—C3—C6—C7 | −67.4 (2) | C11—C10—C17—C16 | −4.0 (3) |
C4—C3—C6—C7 | 171.63 (19) | C9—C10—C17—C16 | 175.98 (17) |
C2—C3—C6—C7 | 52.8 (2) | C13—C16—C17—C10 | −24.5 (3) |
C3—C6—C7—O2 | 151.79 (19) | C13—C16—C17—O1 | 155.55 (16) |
C3—C6—C7—C8 | −30.3 (3) | C8—C9—C18—C24 | −68.8 (2) |
O1—C1—C8—C7 | −177.95 (16) | C10—C9—C18—C24 | 52.3 (2) |
C2—C1—C8—C7 | 1.5 (3) | C8—C9—C18—C19 | 107.97 (19) |
O1—C1—C8—C9 | 4.6 (3) | C10—C9—C18—C19 | −130.94 (18) |
C2—C1—C8—C9 | −175.96 (17) | C24—C18—C19—C20 | 2.5 (3) |
O2—C7—C8—C1 | 179.28 (17) | C9—C18—C19—C20 | −174.21 (17) |
C6—C7—C8—C1 | 1.3 (3) | C18—C19—C20—O5 | 178.32 (18) |
O2—C7—C8—C9 | −3.1 (3) | C18—C19—C20—C22 | −0.9 (3) |
C6—C7—C8—C9 | 178.92 (17) | O5—C20—C22—O4 | −0.8 (3) |
C1—C8—C9—C10 | −10.9 (2) | C19—C20—C22—O4 | 178.46 (18) |
C7—C8—C9—C10 | 171.59 (15) | O5—C20—C22—C23 | 178.72 (17) |
C1—C8—C9—C18 | 111.52 (19) | C19—C20—C22—C23 | −2.0 (3) |
C7—C8—C9—C18 | −65.9 (2) | O4—C22—C23—C24 | −177.13 (18) |
C8—C9—C10—C17 | 10.7 (2) | C20—C22—C23—C24 | 3.3 (3) |
C18—C9—C10—C17 | −111.0 (2) | O4—C22—C23—Br1 | 2.0 (3) |
C8—C9—C10—C11 | −169.39 (16) | C20—C22—C23—Br1 | −177.59 (14) |
C18—C9—C10—C11 | 69.0 (2) | C19—C18—C24—C23 | −1.3 (3) |
C17—C10—C11—O3 | −174.2 (2) | C9—C18—C24—C23 | 175.50 (17) |
C9—C10—C11—O3 | 5.9 (3) | C22—C23—C24—C18 | −1.7 (3) |
C17—C10—C11—C12 | 3.5 (3) | Br1—C23—C24—C18 | 179.19 (14) |
C9—C10—C11—C12 | −176.41 (18) | C8—C1—O1—C17 | 3.6 (2) |
O3—C11—C12—C13 | −156.7 (2) | C2—C1—O1—C17 | −175.94 (15) |
C10—C11—C12—C13 | 25.6 (3) | C10—C17—O1—C1 | −3.8 (3) |
C11—C12—C13—C16 | −50.9 (2) | C16—C17—O1—C1 | 176.09 (15) |
C11—C12—C13—C14 | 70.2 (2) | C19—C20—O5—C21 | 3.2 (3) |
C11—C12—C13—C15 | −168.9 (2) | C22—C20—O5—C21 | −177.50 (19) |