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. 2021 Oct 29;77(Pt 11):1170–1174. doi: 10.1107/S2056989021010690
Bruker Kappa APEX3 CMOS diffractometer 4052 independent reflections
Radiation source: fine-focus sealed tube 3694 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.029
ω and φ scan θmax = 25.0°, θmin = 3.4°
Absorption correction: multi-scan (SADABS; Bruker, 2016) h = −11→11
Tmin = 0.550, Tmax = 0.746 k = −12→12
47600 measured reflections l = −14→14