| Oxford Diffraction Xcalibur, Gemini Ultra R diffractometer | 6870 independent reflections |
| Radiation source: fine-focus sealed X-ray tube | 4304 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.026 |
| Detector resolution: 10.3712 pixels mm-1 | θmax = 32.8°, θmin = 2.2° |
| ω scans | h = −12→10 |
| Absorption correction: analytical [CrysAlisPro (Rigaku OD, 2018), based on expressions derived by Clark & Reid (1995)] | k = −13→14 |
| Tmin = 0.923, Tmax = 0.991 | l = −20→19 |
| 13200 measured reflections |