| Crystal data |
| Chemical formula |
[Co(C9H10N3O2S)2]2(S2O6)·4C3H7NO·3CH4O |
|
M
r
|
1563.53 |
| Crystal system, space group |
Triclinic, P\overline{1} |
| Temperature (K) |
133 |
|
a, b, c (Å) |
13.0652 (8), 14.1171 (9), 19.9233 (12) |
| α, β, γ (°) |
93.179 (2), 106.381 (2), 99.884 (2) |
|
V (Å3) |
3452.2 (4) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.74 |
| Crystal size (mm) |
0.46 × 0.14 × 0.05 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.632, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
51207, 12244, 8043 |
|
R
int
|
0.077 |
| (sin θ/λ)max (Å−1) |
0.596 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.071, 0.203, 1.02 |
| No. of reflections |
12244 |
| No. of parameters |
896 |
| No. of restraints |
7 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.08, −0.66 |
