| Ni1—N5 | 2.100 (4) | N2—C4 | 1.482 (7) |
| Ni1—N5i | 2.100 (4) | O2W—H2WA | 0.8491 |
| Ni1—N2i | 2.070 (4) | O2W—H2WB | 0.8493 |
| Ni1—N2 | 2.070 (4) | C10—H10A | 0.9700 |
| Ni1—N1i | 2.082 (4) | C10—H10B | 0.9700 |
| Ni1—N1 | 2.082 (4) | C10—C9 | 1.528 (8) |
| Ni2—N3ii | 2.069 (4) | N1—H1 | 0.9800 |
| Ni2—N3 | 2.069 (4) | N1—C1 | 1.468 (7) |
| Ni2—N7 | 2.095 (4) | N1—C5i | 1.474 (6) |
| Ni2—N7ii | 2.095 (4) | C3—H3A | 0.9700 |
| Ni2—N4 | 2.079 (4) | C3—H3B | 0.9700 |
| Ni2—N4ii | 2.079 (4) | C3—C2 | 1.512 (8) |
| Ni3—C11 | 1.874 (6) | C4—H4A | 0.9700 |
| Ni3—C11iii | 1.874 (6) | C4—H4B | 0.9700 |
| Ni3—C12iii | 1.857 (6) | C4—C5 | 1.514 (8) |
| Ni3—C12 | 1.857 (6) | O1W—H1WA | 0.8499 |
| Ni4—C13iv | 1.866 (6) | O1W—H1WB | 0.8492 |
| Ni4—C13 | 1.866 (6) | C1—H1A | 0.9700 |
| Ni4—C14iv | 1.863 (6) | C1—H1B | 0.9700 |
| Ni4—C14 | 1.863 (6) | C1—C2 | 1.511 (8) |
| C13—N7 | 1.145 (7) | N4—H4 | 0.9800 |
| N5—C11 | 1.132 (7) | N4—C9 | 1.475 (7) |
| C8—H8A | 0.9700 | C2—H2A | 0.9700 |
| C8—H8B | 0.9700 | C2—H2B | 0.9700 |
| C8—N4 | 1.470 (6) | C6—H6A | 0.9700 |
| C8—C7 | 1.521 (8) | C6—H6B | 0.9700 |
| N8—C14 | 1.156 (7) | C6—C7 | 1.521 (8) |
| N3—H3 | 0.9800 | C5—H5A | 0.9700 |
| N3—C10ii | 1.466 (7) | C5—H5B | 0.9700 |
| N3—C6 | 1.468 (7) | C9—H9A | 0.9700 |
| N6—C12 | 1.154 (7) | C9—H9B | 0.9700 |
| N2—H2 | 0.9800 | C7—H7A | 0.9700 |
| N2—C3 | 1.467 (7) | C7—H7B | 0.9700 |
| C13iv—Ni4—C13 | 180.0 | N3ii—C10—C9 | 109.3 (4) |
| C14iv—Ni4—C13iv | 89.7 (2) | H10A—C10—H10B | 108.3 |
| C14—Ni4—C13iv | 90.3 (2) | C9—C10—H10A | 109.8 |
| C14iv—Ni4—C13 | 90.3 (2) | C9—C10—H10B | 109.8 |
| C14—Ni4—C13 | 89.7 (2) | Ni1—N1—H1 | 107.1 |
| C14iv—Ni4—C14 | 180.0 | C1—N1—Ni1 | 115.1 (3) |
| C11—Ni3—C11iii | 180.0 | C1—N1—H1 | 107.1 |
| C12—Ni3—C11 | 90.1 (2) | C1—N1—C5i | 114.3 (4) |
| C12iii—Ni3—C11iii | 90.1 (2) | C5i—N1—Ni1 | 105.7 (3) |
| C12—Ni3—C11iii | 89.9 (2) | C5i—N1—H1 | 107.1 |
| C12iii—Ni3—C11 | 89.9 (2) | N2—C3—H3A | 109.2 |
| C12iii—Ni3—C12 | 180.0 | N2—C3—H3B | 109.2 |
| N5i—Ni1—N5 | 180.0 | N2—C3—C2 | 111.9 (5) |
| N2—Ni1—N5 | 89.31 (17) | H3A—C3—H3B | 107.9 |
| N2—Ni1—N5i | 90.69 (17) | C2—C3—H3A | 109.2 |
| N2i—Ni1—N5i | 89.31 (17) | C2—C3—H3B | 109.2 |
| N2i—Ni1—N5 | 90.69 (17) | C13—N7—Ni2 | 166.1 (4) |
| N2i—Ni1—N2 | 180.00 (11) | N2—C4—H4A | 109.8 |
| N2—Ni1—N1i | 85.61 (17) | N2—C4—H4B | 109.8 |
| N2i—Ni1—N1 | 85.61 (17) | N2—C4—C5 | 109.6 (5) |
| N2i—Ni1—N1i | 94.39 (17) | H4A—C4—H4B | 108.2 |
| N2—Ni1—N1 | 94.39 (17) | C5—C4—H4A | 109.8 |
| N1i—Ni1—N5 | 90.34 (17) | C5—C4—H4B | 109.8 |
| N1—Ni1—N5 | 89.66 (17) | N6—C12—Ni3 | 176.9 (5) |
| N1i—Ni1—N5i | 89.66 (17) | H1WA—O1W—H1WB | 109.4 |
| N1—Ni1—N5i | 90.34 (17) | N1—C1—H1A | 109.2 |
| N1i—Ni1—N1 | 180.0 | N1—C1—H1B | 109.2 |
| N3ii—Ni2—N3 | 180.0 | N1—C1—C2 | 111.9 (4) |
| N3ii—Ni2—N7ii | 89.44 (17) | H1A—C1—H1B | 107.9 |
| N3—Ni2—N7ii | 90.56 (17) | C2—C1—H1A | 109.2 |
| N3ii—Ni2—N7 | 90.56 (17) | C2—C1—H1B | 109.2 |
| N3—Ni2—N7 | 89.44 (17) | Ni2—N4—H4 | 107.0 |
| N3ii—Ni2—N4 | 85.36 (17) | C8—N4—Ni2 | 115.6 (3) |
| N3—Ni2—N4ii | 85.36 (17) | C8—N4—H4 | 107.0 |
| N3—Ni2—N4 | 94.64 (17) | C8—N4—C9 | 113.8 (4) |
| N3ii—Ni2—N4ii | 94.64 (17) | C9—N4—Ni2 | 105.9 (3) |
| N7ii—Ni2—N7 | 180.0 | C9—N4—H4 | 107.0 |
| N4ii—Ni2—N7ii | 89.87 (17) | C3—C2—H2A | 108.1 |
| N4ii—Ni2—N7 | 90.13 (17) | C3—C2—H2B | 108.1 |
| N4—Ni2—N7ii | 90.13 (17) | C1—C2—C3 | 116.7 (4) |
| N4—Ni2—N7 | 89.87 (17) | C1—C2—H2A | 108.1 |
| N4ii—Ni2—N4 | 180.0 | C1—C2—H2B | 108.1 |
| N7—C13—Ni4 | 176.4 (5) | H2A—C2—H2B | 107.3 |
| C11—N5—Ni1 | 166.1 (4) | N3—C6—H6A | 109.2 |
| H8A—C8—H8B | 107.9 | N3—C6—H6B | 109.2 |
| N4—C8—H8A | 109.2 | N3—C6—C7 | 111.9 (4) |
| N4—C8—H8B | 109.2 | H6A—C6—H6B | 107.9 |
| N4—C8—C7 | 112.1 (5) | C7—C6—H6A | 109.2 |
| C7—C8—H8A | 109.2 | C7—C6—H6B | 109.2 |
| C7—C8—H8B | 109.2 | N1i—C5—C4 | 109.3 (4) |
| Ni2—N3—H3 | 106.9 | N1i—C5—H5A | 109.8 |
| C10ii—N3—Ni2 | 105.8 (3) | N1i—C5—H5B | 109.8 |
| C10ii—N3—H3 | 106.9 | C4—C5—H5A | 109.8 |
| C10ii—N3—C6 | 113.3 (4) | C4—C5—H5B | 109.8 |
| C6—N3—Ni2 | 116.6 (4) | H5A—C5—H5B | 108.3 |
| C6—N3—H3 | 106.9 | C10—C9—H9A | 110.1 |
| Ni1—N2—H2 | 107.0 | C10—C9—H9B | 110.1 |
| C3—N2—Ni1 | 116.2 (3) | N4—C9—C10 | 108.2 (5) |
| C3—N2—H2 | 107.0 | N4—C9—H9A | 110.1 |
| C3—N2—C4 | 113.7 (4) | N4—C9—H9B | 110.1 |
| C4—N2—Ni1 | 105.5 (3) | H9A—C9—H9B | 108.4 |
| C4—N2—H2 | 107.0 | C8—C7—C6 | 117.0 (4) |
| N5—C11—Ni3 | 176.5 (5) | C8—C7—H7A | 108.1 |
| H2WA—O2W—H2WB | 109.4 | C8—C7—H7B | 108.1 |
| N8—C14—Ni4 | 178.0 (5) | C6—C7—H7A | 108.1 |
| N3ii—C10—H10A | 109.8 | C6—C7—H7B | 108.1 |
| N3ii—C10—H10B | 109.8 | H7A—C7—H7B | 107.3 |
| Ni1—N2—C3—C2 | 54.8 (5) | N2—C4—C5—N1i | 56.3 (6) |
| Ni1—N2—C4—C5 | −40.9 (5) | C10ii—N3—C6—C7 | −177.7 (5) |
| Ni1—N1—C1—C2 | −56.5 (5) | N1—C1—C2—C3 | 71.8 (7) |
| Ni2—N3—C6—C7 | −54.5 (5) | C3—N2—C4—C5 | −169.4 (4) |
| Ni2—N4—C9—C10 | −40.9 (5) | C4—N2—C3—C2 | 177.5 (4) |
| C8—N4—C9—C10 | −169.0 (4) | N4—C8—C7—C6 | −70.7 (6) |
| N3ii—C10—C9—N4 | 57.3 (6) | C5i—N1—C1—C2 | −179.1 (4) |
| N3—C6—C7—C8 | 69.7 (6) | C7—C8—N4—Ni2 | 55.4 (5) |
| N2—C3—C2—C1 | −70.5 (7) | C7—C8—N4—C9 | 178.2 (4) |