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. 2021 Oct 21;77(Pt 11):1140–1143. doi: 10.1107/S2056989021010902
Rigaku Xcalibur, Eos diffractometer 3673 independent reflections
Radiation source: fine-focus sealed X-ray tube, Enhance (Mo) X-ray Source 2417 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.036
Detector resolution: 8.0797 pixels mm-1 θmax = 25.0°, θmin = 2.4°
ω scans h = −9→9
Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2018) k = −9→10
Tmin = 0.852, Tmax = 1.000 l = −17→18
7144 measured reflections