| Crystal data |
| Chemical formula |
[Ni2(CN)4(C10H24N4)]·2H2O |
|
M
r
|
457.86 |
| Crystal system, space group |
Triclinic, P\overline{1} |
| Temperature (K) |
180 |
|
a, b, c (Å) |
7.7325 (6), 8.8809 (7), 15.7780 (12) |
| α, β, γ (°) |
88.673 (6), 85.682 (7), 74.623 (7) |
|
V (Å3) |
1041.74 (15) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.83 |
| Crystal size (mm) |
0.30 × 0.20 × 0.06 |
| |
| Data collection |
| Diffractometer |
Rigaku Xcalibur, Eos |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2018 ▸) |
|
T
min, T
max
|
0.852, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
7144, 3673, 2417 |
|
R
int
|
0.036 |
| (sin θ/λ)max (Å−1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.059, 0.159, 1.07 |
| No. of reflections |
3673 |
| No. of parameters |
247 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.31, −0.42 |
