| Crystal data |
| Chemical formula |
C15H18NSe+·HSO4
−·H2O |
|
M
r
|
406.35 |
| Crystal system, space group |
Monoclinic, P21
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
10.4266 (4), 6.0539 (2), 14.2168 (7) |
| β (°) |
90.261 (4) |
|
V (Å3) |
897.38 (6) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
2.23 |
| Crystal size (mm) |
0.22 × 0.18 × 0.16 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD area |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2009 ▸) |
|
T
min, T
max
|
0.624, 0.700 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
4255, 3088, 2624 |
|
R
int
|
0.035 |
| (sin θ/λ)max (Å−1) |
0.649 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.044, 0.113, 0.99 |
| No. of reflections |
3088 |
| No. of parameters |
213 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.40, −0.48 |
| Absolute structure |
Flack x determined using 665 quotients [(I
+)−(I
−)]/[(I
+)+(I
−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
0.002 (16) |
