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. 2021 Oct 19;77(Pt 11):1116–1119. doi: 10.1107/S2056989021010537
U11 U22 U33 U12 U13 U23
Ni1 0.01393 (19) 0.0171 (2) 0.0136 (2) 0.0000 (2) 0.00431 (17) 0.0017 (2)
Ni2 0.0158 (2) 0.0210 (3) 0.0153 (2) −0.0019 (2) 0.00406 (17) −0.0011 (2)
Cl2 0.0180 (4) 0.0431 (7) 0.0155 (4) 0.0016 (4) 0.0057 (3) 0.0037 (4)
Cl3 0.0178 (4) 0.0225 (5) 0.0194 (5) 0.0017 (4) 0.0034 (4) −0.0031 (4)
Cl1 0.0240 (5) 0.0198 (5) 0.0244 (5) −0.0048 (4) 0.0031 (4) 0.0052 (4)
Cl4 0.0301 (5) 0.0180 (5) 0.0367 (7) −0.0042 (4) −0.0027 (5) 0.0021 (5)
O1 0.0275 (15) 0.0233 (17) 0.0205 (16) 0.0014 (13) 0.0077 (13) −0.0051 (13)
N1 0.0159 (14) 0.0249 (19) 0.0133 (16) 0.0017 (13) 0.0054 (13) 0.0017 (14)
N3 0.0163 (13) 0.0206 (17) 0.0170 (15) 0.0001 (15) 0.0056 (12) 0.0000 (16)
N2 0.0122 (13) 0.0204 (19) 0.0200 (18) 0.0019 (13) 0.0044 (13) 0.0019 (14)
O2 0.0186 (14) 0.052 (3) 0.0312 (19) −0.0003 (14) 0.0099 (13) 0.0128 (17)
C8 0.0184 (18) 0.026 (2) 0.020 (2) 0.0079 (16) 0.0113 (16) 0.0058 (17)
C5 0.0221 (18) 0.025 (2) 0.0146 (19) 0.0034 (17) 0.0086 (15) 0.0006 (17)
N6 0.0182 (15) 0.028 (2) 0.0163 (17) 0.0011 (13) 0.0055 (14) −0.0007 (14)
N5 0.029 (2) 0.040 (3) 0.033 (2) −0.0178 (19) −0.0040 (18) 0.020 (2)
C12 0.0200 (18) 0.025 (2) 0.027 (2) −0.0009 (17) 0.0064 (17) 0.0088 (19)
C14 0.0249 (19) 0.033 (3) 0.016 (2) 0.0063 (18) 0.0045 (16) 0.0044 (19)
C3 0.025 (2) 0.036 (3) 0.029 (3) 0.0125 (19) 0.0111 (19) 0.004 (2)
C9 0.032 (2) 0.037 (3) 0.018 (2) 0.011 (2) 0.0145 (18) 0.006 (2)
C1 0.0194 (17) 0.028 (2) 0.019 (2) 0.0006 (16) 0.0077 (15) 0.0024 (17)
C30 0.035 (2) 0.041 (3) 0.033 (3) 0.006 (2) 0.015 (2) 0.000 (2)
N4 0.0223 (18) 0.061 (3) 0.021 (2) 0.0157 (19) 0.0044 (16) −0.005 (2)
C2 0.0149 (17) 0.041 (3) 0.028 (2) 0.0019 (18) 0.0097 (17) 0.007 (2)
C25 0.033 (2) 0.047 (3) 0.031 (3) 0.022 (2) 0.009 (2) −0.001 (2)
C7 0.0174 (16) 0.025 (2) 0.022 (2) 0.0014 (16) 0.0105 (15) 0.0077 (18)
C4 0.025 (2) 0.032 (3) 0.027 (2) 0.0106 (18) 0.0114 (18) 0.002 (2)
C24 0.029 (2) 0.025 (2) 0.017 (2) 0.0080 (18) 0.0041 (18) −0.0052 (18)
C6 0.0243 (19) 0.017 (2) 0.024 (2) 0.0046 (16) 0.0094 (17) −0.0026 (17)
C10 0.030 (2) 0.034 (3) 0.024 (2) 0.007 (2) 0.0142 (18) 0.012 (2)
C23 0.048 (3) 0.015 (2) 0.032 (3) −0.003 (2) 0.001 (2) 0.006 (2)
C15 0.0204 (19) 0.036 (3) 0.028 (2) 0.0014 (18) 0.0032 (18) 0.008 (2)
C31 0.0267 (19) 0.033 (2) 0.032 (2) −0.005 (2) 0.0058 (18) 0.001 (3)
C13 0.0198 (19) 0.040 (3) 0.034 (3) −0.001 (2) 0.0108 (18) 0.010 (2)
C11 0.026 (2) 0.033 (3) 0.035 (3) 0.0008 (19) 0.015 (2) 0.018 (2)
C16 0.033 (2) 0.037 (3) 0.024 (2) 0.009 (2) 0.0120 (19) 0.011 (2)
C18 0.059 (4) 0.067 (4) 0.032 (3) 0.026 (4) 0.003 (3) −0.011 (3)
C17 0.040 (3) 0.057 (4) 0.032 (3) 0.025 (3) −0.004 (2) −0.020 (3)
C26 0.043 (3) 0.047 (4) 0.028 (3) 0.027 (3) 0.005 (2) 0.002 (2)
C21 0.030 (2) 0.091 (5) 0.031 (3) 0.024 (3) 0.013 (2) 0.016 (3)
C28 0.053 (3) 0.029 (3) 0.043 (3) −0.005 (3) −0.002 (3) 0.018 (3)
C32 0.115 (7) 0.050 (4) 0.026 (3) 0.028 (4) 0.016 (4) 0.002 (3)
C22 0.033 (3) 0.113 (7) 0.049 (4) 0.010 (3) 0.020 (3) 0.057 (4)
C27 0.069 (4) 0.029 (3) 0.041 (3) 0.017 (3) −0.004 (3) 0.007 (3)
C29 0.091 (5) 0.027 (3) 0.051 (4) 0.000 (3) −0.007 (4) −0.001 (3)
C19 0.093 (6) 0.071 (5) 0.055 (4) 0.014 (4) 0.044 (4) −0.020 (4)
C20 0.068 (4) 0.104 (6) 0.040 (3) 0.030 (4) 0.025 (3) 0.035 (4)